Abstract

The analysis of in-service lubricating fluids is a useful tool in determining the state of both the fluid and the equipment being lubricated. Many laboratories provide analysis services for in-service lubricating fluids. The results of the analyses performed are often tracked over time to allow for the observation of trends in the test results. The analysis of in-service lubricating grease is a more challenging task; since the amount of grease in many applications is quite small, the grease may be partially or totally replaced each time new grease is added, and access to the lubricated contact zone may be difficult. Many commercial in-service lubricant analysis laboratories lack the specialized test equipment required for grease analysis, so that type of analysis is performed by a limited number of laboratories, primarily those of the grease manufacturers. Various techniques are employed to determine both the macro and micro condition of in-service lubricating grease. The strengths and weaknesses of those techniques are discussed herein.

References

1.
Grease Production Survey 2011, NLGI, Kansas City, MO.
2.
ASTM D217-10
, “
Standard Test Methods for Cone Penetration of Lubricating Grease
,”
Annual Book of ASTM Standards
,
ASTM International
,
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.
3.
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, “
Standard Test Method for Dropping Point of Lubricating Grease over W5de Temperature Range
,”
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,
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,
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4.
American Standard Classification of Lubricating Grease, NLGI, Kansas City, MO.
5.
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,
ASTM International
,
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).
6.
ASTM D1403-10
, “
Standard Test Methods for Cone Penetration of Lubricating Grease Using One-Quarter and One-Half Scale Cone Equipment
,”
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
.
7.
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Standard Test Method for Oxidation Induction Time of Lubricating Greases by Pressure Differential Scanning Calorimetry
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,
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8.
ASTM D7527-10
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Standard Test Method for Measurement of Antioxidant Content of Lubricating Greases by Linear Sweep Voltammetry
,”
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,
ASTM International
,
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9.
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, “
Standard Test Method for Determining Extreme Pressure Properties of Lubricating Greases Using a High-Frequency, Linear-Oscillation (SRV) Test Machine
,”
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
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).
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