Abstract
Modification of a commercially available TG/DTA instrument enabled development of a working TG/DTA/Raman system. The TG/DTA was modified by replacing a portion of the furnace wall above the sample and reference holders with a double layer insulated quartz window. The quartz window provided ready access for Raman spectroscopy, enabling simultaneous collection of TGA, DTA, and Raman data during thermal analytical experiments. Insertion of the quartz glass window did not impact TGA or DTA performance as demonstrated by the comparison of baseline drift and temperature calibration for modified and unmodified furnaces.
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Research Papers
References
1.
2.
3.
Giron
, D.
, Journal of Thermal Analysis and Calorimetry
1418-2874, Vol. 68
, 2002
, pp. 335
-357
.4.
Vora
, A.
, et al, 29th NATAS Conference Proceedings
, 2001
, pp. 101
-105
.5.
Chang
, H.
, et al, Reviews in Analytical Chemistry
, Vol. 20
, No. 3
, 2001
, pp. 207
-238
.6.
Chang
, H.
, et al, Analytical Chemistry
0003-2700 https://doi.org/10.1021/ac960881l, Vol. 69
, 1997
, pp. 1485
-1491
.7.
Huang
, P.
, et al, Thermochimica Acta
0040-6031 https://doi.org/10.1016/S0040-6031(97)00168-8, Vol. 297
, 1997
, pp. 85
-92
.8.
9.
Chang
, H.
, et al, Materials Chemistry and Physics
0254-0584 https://doi.org/10.1016/S0254-0584(98)00239-9, Vol. 58
, 1999
, pp. 12
-19
.10.
Ghule
, A.
, et al, Inorganic Chemistry
0020-1669, Vol. 40
, 2001
, pp. 5917
-5923
.11.
Baskaran
, N.
, et al, Materials Chemistry and Physics
0254-0584 https://doi.org/10.1016/S0254-0584(02)00213-4, Vol. 77
, 2003
, pp. 889
-894
.12.
Murugan
, R.
, et al, Journal of Physics: Condensed Matter
0953-8984 https://doi.org/10.1088/0953-8984/12/5/315, Vol. 12
, 2000
, pp. 677
-700
.13.
Chang
, H.
, et al, Thermochimica Acta
0040-6031 https://doi.org/10.1016/S0040-6031(01)00488-9, Vol. 374
, 2001
, pp. 45
-49
.14.
Murugan
, R.
, et al, Thermochimica Acta
0040-6031 https://doi.org/10.1016/S0040-6031(99)00364-0, Vol. 346
, 2000
, pp. 83
-90
.15.
DuBois
, C.
, et al, 30th NATAS Conference Proceedings
, 2002
, pp. 214
-219
.
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