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ASTM Selected Technical Papers
Techniques in Thermal Analysis: Hyphenated Techniques, Thermal Analysis of the Surface, and Fast Rate Analysis
By
Wei-Ping Pan,
Wei-Ping Pan
1
Western Kentucky University
?Bowling Green, Kentucky Symposium Co-chairman and editor
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Lawrence Judovits
Lawrence Judovits
2
Arkema Inc.
?King of Prussia, Pennsylvania Symposium Co-chairman and editor
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ISBN-10:
0-8031-5616-2
ISBN:
978-0-8031-5616-6
No. of Pages:
142
Publisher:
ASTM International
Publication date:
2007
eBook Chapter
Development and Evaluation of a TG/DTA/Raman System
By
Wendy J. Collins
,
Wendy J. Collins
1
Senior Researcher
, Procter & Gamble Pharmaceuticals
, P.O. Box 191, State Route 320, Norwich, NY 13815
.
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Corey DuBois
,
Corey DuBois
1
Senior Researcher
, Procter & Gamble Pharmaceuticals
, P.O. Box 191, State Route 320, Norwich, NY 13815
.
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R. Thomas Cambron, Ph.D.
,
R. Thomas Cambron, Ph.D.
2
Senior Scientist
, Procter & Gamble Pharmaceuticals
, P.O. Box 191, State Route 320, Norwich, NY 13815
.
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Nancy L. Redman-Furey
,
Nancy L. Redman-Furey
3
Principle Scientist
, Procter & Gamble Pharmaceuticals
, P.O. Box 191, State Route 320, Norwich, NY 13815
.
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Adrienne S. Bigalow Kern
Adrienne S. Bigalow Kern
4
Senior Researcher
, Procter & Gamble Pharmaceuticals
, P.O. Box 191, State Route 320, Norwich, NY 13815
.
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Page Count:
10
-
Published:2007
Citation
Collins, WJ, DuBois, C, Cambron, RT, Redman-Furey, NL, & Bigalow Kern, AS. "Development and Evaluation of a TG/DTA/Raman System." Techniques in Thermal Analysis: Hyphenated Techniques, Thermal Analysis of the Surface, and Fast Rate Analysis. Ed. Pan, W, & Judovits, L. 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959 : ASTM International, 2007.
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Modification of a commercially available TG/DTA instrument enabled development of a working TG/DTA/Raman system. The TG/DTA was modified by replacing a portion of the furnace wall above the sample and reference holders with a double layer insulated quartz window. The quartz window provided ready access for Raman spectroscopy, enabling simultaneous collection of TGA, DTA, and Raman data during thermal analytical experiments. Insertion of the quartz glass window did not impact TGA or DTA performance as demonstrated by the comparison of baseline drift and temperature calibration for modified and unmodified furnaces.
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