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Elemental Analysis of Fossil Fuels and Related Materials
ASTM Monographs
Elemental Analysis of Fossil Fuels and Related Materials
By
Kishore R. A. Nadkarni
Kishore R. A. Nadkarni
Author
1Dr. R. A. Kishore Nadkarni received his Ph.D. in analytical chemistry at the
University of Bombay
.
research associate
at the
University of Kentucky
,
manager
of the
Materials Science Center
?
Analytical Facility
at
Cornell University
, and
analytical leader
in the
ExxonMobil Company
.
member
of the
American Chemical Society
and
ASTM International
. He is very active in
ASTM
and
ISO
in the petroleum products and lubricant field, holding the position of immediate past
chairman
of ISO/TC28,
chairman
of ASTM's D02.03 on Elemental Analysis,
vice-chairman
of D02.92 on Proficiency Test Programs, D02.94 on Quality Assurance and Statistics.
Search for other works by this author on:
This Site
PubMed
Google Scholar
ISBN:
978-0-8031-7044-5
No. of Pages:
900
DOI:
https://doi.org/10.1520/MONO10-EB
Publisher:
ASTM International
Publication date:
2014
eBook Chapter

Elemental Analysis of Coal, Coke, and Fly Ash

Doi:
https://doi.org/10.1520/MONO102012000805
Page Count:
147
  • Published:
    2014

Elemental analysis of coal, coke, fly ash, and related products is discussed in detail with examples of multi-element multi-technique analysis of these products.

Keywords:
elemental analysis, coal, coke, fly ash, mercury, sulfur, radioactivity

References

1.
Dunham
,
J. T.
,
Rampacek
,
C.
, and
Henrie
,
T. A.
, “
High Sulfur Coal for Generating Electricity
,”
Science
, Vol.
184
,
1974
, pp. 346–350.
2.
Janke
,
L. C. G.
,
Lupens
,
J. A.
, and
Graham
,
R. D.
,
ASTM Standardization News
, Vol.
32
,
2004
, pp. 22–27.
3.
Bertine
,
K. K.
, and
Goldberg
,
R. D.
, “
Fossil Fuel Combustion and the Major Sedimentary Cycle
,”
Science
, Vol.
173
,
1971
, pp. 233–235.
4.
Osborn
,
E. F.
, “
Coal and the Present Energy Situation
,”
Science
, Vol.
183
,
1974
, pp. 477–481.
5.
Walsh
,
J.
, “
Problems of Expanding Coal Production
,”
Science
, Vol.
184
,
1974
, pp. 336–339.
6.
Squires
,
A. M.
, “
Clean Fuels from Coal Gasification
,”
Science
, Vol.
184
,
1974
, pp. 340–346.
7.
Fancher
,
J. R.
, “
Trace Element Emissions from the Combustion of Fossil Fuels
,” in
Cycling and Control of Metals
,
National Environmental Research Center
,
Cincinnati, OH
,
1973
, pp. 109–114.
8.
“
Outlook
,”
Environ. Sci. Technol.
, Vol.
9
,
1975
, pp. 18–24.
9.
Rubin
,
E. S.
, and
McMichael
,
F. C.
, “
Impact of Regulations on Coal Conversion Plants
,”
Environ. Sci. Technol.
, Vol.
9
,
1975
, pp. 112–117.
10.
Klein
,
D. H.
, and
Russell
,
P.
, “
Heavy Metals. Fallout Around a Power Plant
,”
Environ. Sci. Technol.
, Vol.
7
,
1973
, pp. 357–358.
11.
Capes
,
C. E.
,
McLlhinney
,
A. E.
,
Russell
,
D. S.
, and
Sirianni
,
A. F.
, “
Rejection of Trace Metals from Coal during Beneficiation by Agglomeration
,”
Environ. Sci. Technol
., Vol.
8
,
1974
, pp. 35–38.
12.
Bloomberg News, Star Ledger, Newark, NJ, p. 8, Dec. 31,
2011
.
13.
Johnson
,
J.
, “
EPA Ruling on Coal Burning Power Plants
,” Chem. Engr. News,
2012
, p. 10.
14.
Ray
,
S. S.
, and
Parker
,
F. G.
, Characterization of Ash from Coal-Fired Power Plants, EPA-600.7-77-010,
Office of Energy, Minerals, and Industry, U.S. Environmental Protection Agency
, Washington, DC,
1977
.
15.
Lyon
,
W. S.
,
Trace Element Measurements at the Coal-Fired Steam Plant
,
CRC Press
,
Cleveland, OH
,
1977
.
16.
Natusch
,
D. F. S.
,
Walker
,
J. R.
, and
Evans
,
C. A.
, Jr., “
Toxic Trace Elements: Preferential Concentration in Respirable Particles
,”
Science
, Vol.
183
,
1974
, pp. 202–204.
17.
Kaakinen
,
J. F.
,
Jorden
,
R. M.
,
Lawasani
,
M. H.
, and
West
,
R. E.
, “
Trace Element Behavior in Coal-Fired Power Plant
,”
Environ. Sci. Technol.
, Vol.
9
,
1975
, pp. 862–869.
18.
Meserole
,
F. B.
,
Schwitzgebel
,
K.
,
Magee
,
R. A.
, and
Mann
,
R. W.
, ASME Paper No. 78-WA/Fu-9,
1978
.
19.
Cavallaro
,
J. A.
,
Deurbrouch
,
A. W.
,
Schultz
,
H.
,
Gibbon
,
G. A.
, and
Hattman
,
E. A.
, A Washability and Analytical Evaluation of Potential Pollution from Trace Elements in Coal, EPA-600/7-78-038,
Office of Energy, Minerals, and Industry, U.S. Environmental Protection Agency
, Washington, DC,
1978
.
20.
Ondov
,
J. M.
,
Ragaini
,
R. C.
, and
Biermann
,
A. H.
, “
Elemental Emissions from a Coal-Fired Power Plant. Comparison of a Venturi Wet Scrubber System with a Cold-Side Electrostatic Precipitator
,”
Environ. Sci. Technol.
, Vol.
13
,
1979
, pp. 598–607.
21.
Task Group on Lung Dynamics
, “
Deposition and Retention Models for Internal Dosimetry of the Human Respiratory Tract
,”
Health Physics
, Vol.
12
,
1966
, pp. 173–207.
22.
Davison
,
R. L.
,
Natusch
,
D. F. S.
,
Wallace
,
J. R.
, and
Evans
, ,
C. A.
 Jr., “
Trace Elements in Fly Ash. Dependence of Concentration on Particle Size
,”
Environ. Sci. Technol
., Vol.
8
,
1974
, pp. 1107–1113.
23.
Fisher
,
G. L.
,
Change
,
D. P. Y.
, and
Brummer
,
M.
, “
Fly Ash Collected from Electrostatic Precipitators: Microcrystalline Structures and the Mystery of the Spheres
,”
Science
, Vol.
192
,
1976
, pp. 553–555.
24.
Campbell
,
J. A.
,
Laul
,
J. C.
,
Nielson
,
K. K.
, and
Smith
,
R. D.
, “
Separation and Chemical Characterization of Finely-Sized Fly-Ash Particles
,”
Anal. Chem.
, Vol.
50
,
1978
, 1032–1040.
25.
Biermann
,
A. H.
, and
Ondov
,
J. M.
, UCRL-81361,
1978
.
26.
Natusch
,
D. F. S.
, WPA-600/9-78, 0206,
1978
.
27.
Lee
, ,
R. E.
 Jr., and
Von Lehmden
,
D. J.
, “
Trace Metal Pollution in the Environment
,”
J. Air Poll. Control. Assoc.
, Vol.
23
,
1973
, pp. 853–857.
28.
Toca
,
F. M.
,
Diss. Abstr. Int.
,
33
, 3156B,
1973
.
29.
Straughan
,
I.
,
Elseewi
,
A. A.
, and
Page
,
A. L.
, “
Mobilization of Selected Trace Elements in Residues
,” in
Proceedings of the 12th Conference on Trace Substances in Environmental Health XII Symposium
,
University of Missouri
,
Columbia, MO
,
1979
, pp. 389–402.
30.
Messerole
,
F. B.
,
Schwitzgebel
,
K.
,
Magee
,
R. A.
, and
Mann
,
R. M.
, Amer. Soc. Mech. Engr., 78-WA/FU-9,
1978
.
31.
Smith
,
R. D.
,
Campbell
,
J. A.
, and
Nielson
,
K. K.
, “
Concentration Dependence upon Particle Size of Volatilized Elements in Fly Ash
,”
Environ. Sci. Technol.
, Vol.
13
,
1979
, pp. 553–558.
32.
Henry
,
W. M.
, and
Knapp
,
K. T.
, “
Compound Forms of Fossil Fuel Fly Ash Emissions
,”
Environ. Sci. Technol.
, Vol.
14
,
1980
, pp. 450–456.
33.
Coles
,
D. G.
,
Ragini
,
R. C.
,
Ondov
,
J. M.
,
Fisher
,
G. L.
,
Silberman
,
D.
, and
Prentice
,
B. A.
, “
Chemical Studies of Stack Fly Ash from a Coal-Fired Power Plant
,”
Environ. Sci. Technol.
, Vol.
13
,
1979
, pp. 455–459.
34.
Weissman
,
S. H.
,
Carpenter
,
R. L.
, and
Newton
,
G. J.
, “
Respirable Aerosols from Fluidized Bed Coal Combustion. 3. Elemental Composition of Fly Ash
,”
Environ. Sci. Technol.
, Vol.
17
,
1983
, pp. 65–71.
35.
Rao
,
C. P.
, and
Gluskoter
,
H. J.
, “
Occurrence and Distribution of Minerals in Illinois Coals
,” in
Illinois State Geological Survey Circular
,
No. 476
,
Illinois State Geological Survey, Urbana, IL
,
1973
.
36.
O'Gorman
,
J. V.
, and
Walker
,
P. L.
, Jr., Mineral Matter and Trace Elements in U.S. Coals, Research and Development Report No. 61, Interim Report No. 2,
Office of Coal Research, U.S. Department of Interior
, Washington, DC,
1972
, p. 184.
37.
Gluskoter
,
H. J.
, “
Mineral Matter and Trace Elements in Coal
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series Vol.
141
,
American Chemical Society
,
Washington, DC
,
1974
, pp. 1–22.
Google Scholar
Crossref
Search ADS
 
38.
Given
,
P. H.
, “
An Essay on the Organic Geochemistry of Coal
,” in
Coal Science
,
Gorbaty
 
M. L.
,
Larsen
 
J. W.
, and
Wender
 
E.
, Eds.,
Academic Press
,
Orlando, FL
, Vol.
3
, p. 76.
Crossref
Search ADS
 
39.
Von Lehmeden
,
D. J.
,
Jungers
,
R. H.
, and
Lee
,
R. E.
, “
Determination of Trace Elements in Coal, Fly Ash, Fuel Oil, and Gasoline. Preliminary Comparison of Selected Analytical Techniques
,”
Anal. Chem.
, Vol.
46
,
1974
, pp. 239–245.
40.
Nadkarni
,
R. A.
, “
Multitechnique Multielement Analysis of Coal and Fly Ash
,”
Anal. Chem.
, Vol.
52
,
1980
, pp. 929–935.
41.
Riley
,
J. T.
,
Routine Coal and Coke Analysis
, Manual 57,
ASTM International
,
West Conshohocken, PA
,
2007
.
42.
Wiser
,
W. H.
, “
Mechanisms of Coal Liquefaction
,”
Proceedings of the Department of Energy Report Review Meeting
, June 8,
1978
, p. 4.
43.
Slates
,
R. V.
, Dupont Report, OP-1421,
1976
.
44.
Babu
,
S. P.
,
Trace Elements in Fuel
,
American Chemical Society
,
Washington, DC
,
1975
.
Google Scholar
Crossref
Search ADS
 
45.
Karr
,
C. K.
, Jr.,
Analytical Methods for Coal and Coal Products
, Vol.
1
,
Academic Press
,
New York
,
1978
.
46.
Nadkarni
,
R. A.
,
Guide to ASTM Test Methods for the Analysis of Coal and Coke
, Manual 61,
ASTM International
,
West Conshohocken, PA
,
2008
.
Google Scholar
Crossref
Search ADS
 
47.
Ode
,
W. H.
, “
Coal Analysis and Mineral Matter
,” in
Chemistry of Coal Utilization
,
Lowry
 
H.
, Ed.,
Supplementary
Volume,
Wiley
,
New York
,
1963
, p. 204.
48.
Montgomery
,
W. J.
, “
Standard Laboratory Test Methods for Coal and Coke
,” in
Analytical Methods for Coal and Coal Products
, Vol.
1
,
Academic Press
,
New York
,
1978
, p. 205.
Google Scholar
Crossref
Search ADS
 
49.
Nadkarni
,
R. A.
,
Spectroscopic Analysis of Petroleum Products and Lubricants
, MONO 9,
ASTM International
,
West Conshohocken, PA
,
2011
.
Google Scholar
Crossref
Search ADS
 
50.
Robertson
,
D. E.
, “
Role of Contamination in Trace Element Analysis of Sea Water
,”
Anal. Chem.
, Vol.
40
,
1968
, pp. 1067–1072.
51.
Zief
,
M.
, and
Mitchell
,
J. W.
,
Contamination Control in Trace Element Analysis
,
John Wiley
,
New York
,
1976
.
52.
Strumpler
,
A. W.
,
Anal. Chem.
, Vol.
45
,
1973
, p. 2251.
53.
Shendrikar
,
A. D.
,
Dharmarajan
,
V.
,
Walker-Merrick
,
H.
, and
West
,
P. W.
, “
Adsorption Characteristics of Traces of Barium, Beryllium, Cadmium, Manganese, Lead and Zinc on Selected Surfaces
,”
Anal. Chim. Acta
, Vol.
84
,
1976
, pp. 409–417.
54.
Nadkarni
,
R. A.
, and
Brewer
,
J. M.
, “
Semiquantitative Proximate Analysis of Fossil Fuels
,”
Amer. Lab.
, Vol.
19
,
1987
, pp. 87–95.
55.
Nadkarni
,
R. A.
, “
Alternatives to ASTM Tests for Rapid Coal Analysis
,” in
Proceedings of the 3rd International Coal Testing Conference
, Vol.
3
,
Lexington, KY
,
1983
, pp. 135–142.
56.
Fabbi
,
B. P.
, and
Espoa
,
L. P.
, USGS Professional Paper, 840, 89,
1976
.
57.
National Bureau of Standards Certificate of Analysis,
1978
.
58.
Fruchter
,
J. S.
,
Wilkerson
,
C. L.
,
Evans
,
J. C.
, and
Sanders
,
R. W.
, “
Elemental Partitioning in an Aboveground Oil Shale Retort Pilot Plant
,”
Environ. Sci Technol.
, Vol.
14
,
1980
, pp. 1374–1381.
59.
Flanagan
,
F. J.
, “
1972 Values for International Geochemical Reference Samples
,”
Geochim. Cosmochim. Acta
, Vol.
37
,
1973
, 1189–1200.
60.
Riley
,
J. T.
,
Ruba
,
G. M.
, and
Lee
,
C. C.
, “
Direct Determination of Organic Sulfur
,” in
Geochemistry of Sulfur in Fossil Fuels
,
Orr
 
W. L.
 and
White
 
C. M.
, Eds., ACS Symposium Series No. 429, Chapter 13,
American Chemical Society
,
Washington, DC
,
1990
.
61.
Edwards
,
A. H.
,
Daybell
,
G. N.
, and
Pringle
,
W. J. S.
, “
An Investigation into Methods for the Determination of Forms of Sulfur in Coal
,”
Fuel
, Vol.
37
,
1958
, pp. 47–59.
62.
Burns
,
M. S.
, “
Determination of Pyritic Sulfur in Australian Coals
,”
Fuel
, Vol.
49
,
1970
, pp. 126–133.
63.
Neavel
,
R. C.
, in
Chemistry of Coal Utilization
,
Elliott
 
M. A.
, Ed.,
John Wiley and Sons
,
New York
,
1981
, p. 91.
64.
Nadkarni
,
R. A.
,
Cornett
,
R. B.
, and
Bredweg
,
R. L.
, “
Evaluation of an Elemental Analyzer
,”
Amer. Lab.
,
17
(
2
), 69–81,
1985
.
65.
James
,
W. D.
,
Ehmann
,
W. D.
,
Hamrin
,
C. E.
, and
Chyi
,
L. L.
, “
Oxygen and Nitrogen in Coal by Instrumental Neutron Activation Analysis
,”
J. Radioanal. Chem.
, Vol.
32
, pp. 195–205.
66.
Chyi
,
L. L.
,
James
,
W. D.
,
Ehmann
,
W. D.
,
Sun
,
G. H.
, and
Hamrin
,
C. E.
,
Proceed. Sci. Ind. Appl. Small Accelerators
, Vol.
4
,
1976
, p. 281.
67.
Hamrin
,
C. E.
,
Maa
,
P. S.
,
Chyi
,
L. L.
, and
Ehmann
,
W. D.
,
Fuel
, Vol.
58
,
1979
, p. 48.
68.
Gluskoter
,
H. J.
,
Ruch
,
R. R.
,
Miller
,
W. G.
,
Cahill
,
R. A.
,
Dreher
,
G. B.
, and
Kuhn
,
J. K.
, Illinois State Geological Survey Circular, 499,
1977
.
69.
Filby
,
R. H.
, and
Khalil
,
S. R.
,
Symp. Potential Health Environ, Effects of Synth. Fuel Technologies
,
Gatlinberg, TN
,
1978
.
70.
Kuhn
,
J. K.
,
Fiene
,
F. L.
,
Cahill
,
R. A.
,
Gluskoter
,
H. J.
, and
Shimp
,
N. F.
, Environ. Geol. Notes, 88,
1980
.
71.
Buenafama
,
H. D.
, “
Nuclear Methods for Trace Elements in Petroleum and Petroleum Products
,” in
Atomic and Nuclear Methods in Fossil Energy Research
,
Plenum Press
,
New York
,
1982
, pp. 29–44.
Google Scholar
Crossref
Search ADS
 
72.
Volborth
,
A.
, in
Analytical Methods for Coal and Coal Products
,
Karr
 
C.
, Ed.,
Academic Press
,
New York
,
1979
, Vol.
3
, p. 303.
73.
Khalil
,
S. R.
,
Koppenaal
,
D. W.
, and
Ehmann
,
W. D.
,
J. Radioanal. Nucl. Chem.
, Vol.
57
,
1980
, p. 195.
74.
Hamrin
,
C. E.
,
Johannes
,
A. H.
,
James
,
W. D.
,
Sun
,
G. H.
, and
Ehmann
,
W. D.
, “
Determination of Oxygen and Nitrogen in Coal by Instrumental Neutron Activation Analysis
,”
Fuel
, Vol.
58
,
1979
, pp. 48–54.
75.
Nadkarni
,
R. A.
, “
Comprehensive Elemental Analysis of Coal and Fly Ash
,” in
Coal and Coal Products: Analytical Characterization Techniques
,
Fuller
,
E. L.
 Jr., Ed., American Chemical Society Symposium Series Vol.
205
,
American Chemical Society
,
Washington, DC
,
1982
, pp. 147–162.
76.
Nadkarni
,
R. A.
, and
Botto
,
R. I.
, “
Analysis of National Bureau of Standards Fossil Fuel Standard Reference Materials
,”
J. Coal Qual.
, Vol.
5
,
1986
, pp. 67–71.
77.
O'Reilly
,
J. E.
, and
Hicks
,
D. G.
, “
Slurry-Injection Atomic Absorption Spectrometry for Analysis of Whole Coal
,”
Anal. Chem.
, Vol.
51
,
1979
, pp. 1905–1915.
78.
Ebdon
,
E.
, and
Parry
,
H. G. M.
, “
Determination of Major, Minor, and Trace Elements in Coal Slurries by Direct Current Plasma-Atomic Emission
,”
Microchem. J.
, Vol.
41
,
1990
, pp. 219–226.
79.
Ng
,
K. C.
, Zerezghi, and
Caruso
,
J. A.
, “
Direct Powder Injection of NBS Coal Fly Ash in Inductively Coupled Plasma Atomic Emission Spectrometry with Rapid Scanning Spectrometric Detection
,”
Anal. Chem.
, Vol.
56
,
1984
, pp. 417–424.
80.
Gehlhausen
,
J. M.
, and
Carnahan
,
J. W.
, “
Simultaneous Determination of Elemental Ratios in Coal by Direct Powder Injection into a Helium Microwave Induced Plasma
,”
Anal. Chem.
, Vol.
63
,
1991
, pp. 2430–2434.
81.
Ebdon
,
L.
, and
Wilkinson
,
J. R.
, “
Direct Atomic Spectrometric Analysis by Slurry Atomisation. Part 1. Optimisation of Whole Coal Analysis by Inductively Coupled Plasma Atomic Emission Spectrometry
,”
J. Anal. At. Spectrom.
, Vol.
2
,
1987
, pp. 39–44.
82.
Ebdon
,
L.
, and
Wilkinson
,
J. R.
, “
Direct Atomic Spectrometric Analysis by Slurry Atomisation. Part 3. Whole Coal Analysis by Inductively Coupled Plasma Atomic Emission Spectrometry
,”
J. Anal. At. Spectrom.
Vol.
2
,
1987
, pp. 325–328.
83.
McCurdy
,
D. L.
,
Wichman
,
M. D.
, and
Fry
,
R. C.
, “
Rapid Coal Analysis. Part II: Slurry Atomization DCP Emission Analysis of NBS Coal
,”
Appl. Spectr.
, Vol.
39
,
1985
, pp. 984–988.
1985
.
84.
McCurdy
,
D. L.
, and
Fry
,
R. C.
, “
Rapid Sulfur Determination in Bituminous and Subbituminous Coal by Slurry Atomization Inductively Coupled Plasma Emission Spectrometry
,”
Anal. Chem.
, Vol.
58
,
1986
, pp. 3126–3132.
85.
Brenner
,
I. B.
, and
Zander
,
A.
, “
Sequential Multielement Analysis of Coals by Slurry Nebulization Using Ar, Ar-O2, and N2 Inductively Coupled Plasma Atomic Emission Spectrometry
,”
Spectroscopy
, Vol.
13
,
1998
, pp. 14–23.
86.
O'Reilly
,
J. E.
, and
Hale
,
M. A.
, “
Direct Atomic Absorption Analysis of Powdered Whole-Coal Slurries
,”
Anal. Lett.
, Vol.
10
,
1977
, pp. 1095–1104.
87.
O'Reilly
,
J. E.
, and
Hicks
,
D. G.
, “
Slurry-Injection Atomic Absorption Spectrometry for Analysis of Whole Coal
,”
Anal. Chem.
, Vol.
51
,
1979
, pp. 1905–1915.
88.
Riley
,
J. T.
,
Werth
,
J. L.
,
Lewis
,
L. M.
, and
Mertens
,
M. J.
, “
ICP Analysis of Coal Slurries
,” in
Elemental Analysis of Coal and Its By-Products
,
Vourvopoulos
 
G.
, Ed.,
World Scientific Publishing Co.
,
River Edge, NJ
,
1992
, pp. 124–144.
89.
Renfrow
,
M. B.
,
Riley
, ,
J. M.
 Jr., and
Riley
,
J. T.
, “
AICP-Atomic Emission Spectrometric Analysis of Aqueous Slurries of Solids
,”
Microchem.
J., Vol.
56
,
1997
, pp. 30–39.
90.
Spielholtz
,
G. I.
, and
Diehl
,
H.
, “
Wet Ashing of Coal with Perchloric Acid Mixed with Periodic Acid for the Determination of Sulphur and Certain Other Constituents
,”
Talanta
, Vol.
13
,
1966
, pp. 991–1002.
91.
Capes
,
C. E.
,
McIlhinney
,
A. E.
,
Russell
,
D. S.
, and
Sirianni
,
A. F.
, “
Rejection of Trace Metals from Coal during Beneficiation by Agglomeration
,”
Environ. Sci. Technol.
, Vol.
8
,
1974
, pp. 35–38.
92.
Ward
,
A. F.
, and
Marciello
,
L.
, “
Analysis of Energy Resources by ICAP Spectroscopy: Petroleum Products
,”
Jarrell Ash Plasma Newslett.
Vol.
1
,
1978
, pp. 10–14.
93.
Hartstein
,
A. M.
,
Freedman
,
R. W.
, and
Platter
,
D. W.
, “
Novel Wet-Digestion Procedure for Trace Metal Analysis of Coal by Atomic Absorption
,”
Anal. Chem.
, Vol.
45
, pp. 611–614.
94.
Dreher
,
G. B.
, and
Schleicher
,
J. A.
, “
Trace Elements in Coal by Optical Emission Spectroscopy
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
American Chemical Society
,
Washington, DC
,
1975
, pp. 35–47.
Google Scholar
Crossref
Search ADS
 
95.
Ruch
,
R. R.
,
Gluskoter
,
H. J.
, and
Shimp
,
N. F.
, Ill. State Geol. Survey, Environ. Geol. Notes, 72,
1974
.
96.
Werverka
,
E. M.
, and
Williams
,
J. M.
, LA-6835-PR,
1978
.
97.
Kelly
,
W. R.
, and
Moore
,
C. B.
, “
Determination of Trace Elements in Coal and Coal Ash by Spark Source Mass Spectrometry
,”
Anal. Chem.
, Vol.
45
,
1973
, pp. 1275–1277.
98.
Pollock
,
E. N.
, ACS Divn. Fuel Chem. Preprints, 18, 92,
1973
.
99.
Pollock
,
E. N.
, “
Trace Impurities in Coal by Wet Chemical Methods
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
American Chemical Society
,
Washington, DC
,
1975
, pp. 23–34.
Google Scholar
Crossref
Search ADS
 
100.
Pradhan
,
N. K.
,
Coal and Petroleum Analysis by Atomic Absorption Spectrometry
,
Varian Techtron
,
Melbourne, Australia
,
1976
.
101.
Kometani
,
T. Y.
,
Bove
,
J. L.
,
Nathanson
,
B.
,
Siebenberg
,
S.
, and
Magyar
,
M.
, “
Dry Ashing of Airborne Particulate Matter on Paper and Glass Fiber Filters for Trace Metal Analysis by Atomic Absorption Spectrometry
,”
Environ. Sci. Technol
., Vol.
6
,
1972
, pp. 617–620.
102.
Lee
,
S. H. D.
,
Johnson
,
I.
, and
Fisher
,
J.
, ANL/CEN/FE-77-4,
1977
.
103.
Heinricjs
,
H.
, “
Emissions of 22 Elements from Brown-Coal Combustion
,”
Naturwiss.
, Vol.
64
,
1977
, pp. 479–481.
104.
Santoliquido
,
P. M.
,
Radiochem. Radioanal. Lett.
, Vol.
15
,
1973
, p. 373.
105.
Frost
,
J. K.
,
Santoliquido
,
P. M.
,
Camp
,
L. R.
, and
Ruch
,
R. R.
, “
Trace Elements in Coal by Neutron Activation Analysis with Radiochemical Separations
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
American Chemical Society
,
Washington, DC
,
1975
, pp. 84–97.
Google Scholar
Crossref
Search ADS
 
106.
Gluskoter
,
H. J.
,
Fuel
, Vol.
44
,
1965
, p. 285.
107.
Lutz
,
G. J.
,
Stemple
,
J.
, and
Rook
,
H. L.
, “
Evaluation by Activation Analysis of Elemental Retention in Biological Samples after Low Temperature Ashing
,”
J. Radioanal. Nucl. Chem.
, Vol.
39
,
1977
, pp. 277–283.
108.
Gleit
,
C. E.
, and
Holland
,
W. D.
, “
Use of Electrically Excited Oxygen for the Low Temperature Decomposition of Organic Substances
,”
Anal. Chem.
, Vol.
34
,
1962
, pp. 1454–1457.
109.
O'Gorman
,
J. V.
,
Suhr
,
N. H.
, and
Walker
,
P. L.
, “
The Determination of Mercury in Some American Coals
,”
Appl. Spectr.
, Vol.
26
,
1972
, pp. 44–48.
110.
Miller
,
R. N.
,
Yarzab
,
R. F.
, and
Given
,
P. H.
, “
Determination of the Mineral-Matter Contents of Coals by Low-Temperature Ashing
,”
Fuel
, Vol.
58
,
1979
, pp. 4–10.
111.
Karacki
,
S. S.
, and
Corcoran
,
F. L.
, “
Coal Ash Analysis with an Argon Plasma Emission Excitation Source
,”
Appl. Spectr.
, Vol.
27
,
1973
, pp. 41–42.
112.
Muter
,
R. B.
, and
Nice
,
L. L.
, “
Major and Minor Constituents in Siliceous Materials by Atomic Absorption Spectrometry
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
American Chemical Society
,
Washington, DC
,
1975
, pp. 57–65.
113.
Boar
,
P. L.
, and
Ingram
,
L. K.
, “
The Comprehensive Analysis of Coal Ash and Silicate Rocks by Atomic-Absorption Spectrophotometry by a Fusion Technique
,”
Analyst
, Vol.
95
,
1970
, pp. 124–130.
114.
Schultz
,
H.
,
Hattman
,
E. A.
, and
Booher
,
W. B.
, “
Trace Element Mass Balance Around a Coal-Fired Steam Plant
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
American Chemical Society
,
Washington, DC
,
1975
, pp. 139–153.
115.
Botto
,
R. I.
,
Jarrell Ash Plasma News.
, Vol.
2
,
1979
, pp. 4–8.
116.
Bernas
,
B.
, “
New Method for Decomposition and Comprehensive Analysis of Silicates by Atomic Absorption Spectrometry
,”
Anal. Chem
., Vol.
40
,
1968
, pp. 1682–1686.
117.
Kotz
,
L.
,
Kaiser
,
G.
, Tschopel, and
Tolg
,
G., Z.
,
Anal. Chem.
, Vol.
260
,
1972
, p. 207.
118.
Gallorini
,
M.
,
Greenberg
,
R. R.
, and
Gills
,
T. E.
, “
Simultaneous Determination of Arsenic, Antimony, Cadmium, Chromium, Copper, and Selenium in Environmental Material by Radiochemical Neutron Activation Analysis
,”
Anal. Chem.
, Vol.
50
, pp. 1479–1481.
119.
Van Eenbergen
,
A.
, and
Bruninx
,
E.
, “
Losses of Elements during Sample Decomposition in an Acid-Digestion Bomb
,”
Anal. Chim. Acta
, Vol.
98
,
1978
, pp. 405–406.
120.
Nadkarni
,
R. A.
, “
Applications of Microwave Oven Sample Dissolution in Analysis
,”
Anal. Chem.
, Vol.
56
,
1984
, pp. 2233–2237.
121.
General Electric, Co., “
Coal Desulfurization System by Crushing and Microwave Irradiation with Specified Parameters
,” U.S. Patent 4,076,607,
1978
.
122.
Zavitsanos
,
P. D.
,
Bleiler
,
K. W.
,
Golden
,
J. A.
, and
Kinkead
,
W. K.
, Coal Desulfurization Using Microwave Energy, Final Report, EPA-68-02-2172,
U.S. Environmental Protection Agency
, Washington, DC,
1979
.
123.
Kirkbride
,
C. G.
, “
Desulfurization of Coal by Microwave Treatment in a Hydrogen Atmosphere
,” U.S. Patent, 4,123,230,
1978
.
124.
Kirkbride
,
C. G.
, and
Chalmer
,
G.
, “
Removing Sulfur from Coal
,” U.S. Patent 4,148,614,
1979
.
125.
Judzis
,
A.
, Jr.,
Hiatt
,
R. E.
, and
Williams
,
B.
, “
Use of Microwaves in Measuring the Organic Content of Oil Shale
,”
Proceed. IEEE
, Vol.
65
,
1977
, pp. 1626–1627.
126.
Judzias
,
A.
, “
Analyzing Green River Oil Shale with Microwave Radiation
,”
Diss. Abstr. Int. B
, Vol.
39
N.
2 874B
,
1978
.
127.
Nottenburg
,
R. N.
,
Rajeshwar
,
K.
,
Rosenvold
,
R. J.
, and
DuBow
,
J. B.
, “
Temperature and Stress Dependence of Electrical and Mechanical Properties of Green River Oil Shale
,”
Fuel
, Vol.
58
,
1979
, pp. 144–148.
128.
Rajeshwar
,
K.
,
Nottenburg
,
R.
,
DuBow
,
J.
, and
Rosenvold
,
R.
, “
Electrical Conduction Mechanism in Green River Shale
,”
Thermochim. Acta
, Vol.
27
,
1978
, pp. 357–360.
129.
Rajeshwar
,
K.
,
Nottenburg
,
R.
, and
DuBow
,
J.
, “
Review of Thermophysical Properties of Oil Shale
,”
J. Materials Sci.
, Vol.
14
,
1979
, pp. 2025–2052.
130.
Rhys
,
H. R.
, “
Separating Nahcolite Particles from Oil Shale Particles Involves Wetting Particles and Subjecting Them to Microwave Energy to Whiten Nahcolite
,” U.S. Patent 3,992,287,
1976
.
131.
Abu-Samra
,
A.
,
Morris
,
J. S.
, and
Koirtyohann
,
S. R.
, “
Wet Ashing of Some Biological Samples in a Microwave Oven
,”
Anal. Chem.
, Vol.
47
,
1975
, pp. 1475–1477.
132.
Barrett
,
P.
,
Davidowski
,
L. J.
,
Penaro
,
K. W.
, and
Copeland
,
T. R.
, “
Microwave Oven-Based Wet Digestion Technique
,”
Anal. Chem.
, Vol.
50
,
1978
, pp. 1021–1023.
133.
West
,
M. H.
,
Mollina
,
J. F.
,
Yuan
,
C. L.
,
Davis
,
D. G.
, and
Chauvin
,
J. V.
,
Anal. Chem.
, Vol.
51
,
1979
, p. 2370.
134.
Matthes
,
S. A.
,
Farrell
,
R. F.
, and
Mackie
,
A. J.
, Technical Progress Report, 120,
U.S. Bureau of Mines
, Washington, DC,
1983
.
135.
Williams
,
R. B.
, and
Nadkarni
,
R. A.
, “
Use of Electromagnetic Radiation to Recover Alkali Metal Constituents from Coal Conversion Residues
,” U. S. Patent 3,365,975,
1982
.
136.
Nadkarni
,
R. A.
, and
Williams
,
R. B.
, “
Coal and Oil Shale Beneficiation Process
,” U.S. Patent 4,408,999,
1983
.
137.
Guzenda
,
D.
, and
Zielinski
,
W.
 “
Attempt of a Application of a Microwave Method to Determine Moisture Content in Coal Fines
,”
Zesz. Nauk. Akad. Gorn. Hutn. Cracow Gorn
, Vol.
87
,
1976
, pp. 125–130.
138.
Hall
,
D. A.
,
Sproson
,
J. C.
, and
Gray
,
W. A.
, “
Rapid Determination of Moisture in Coal Using Microwaves
,” J. Inst. Fuel, 43, 350, 354,
1970
.
139.
Ryley
,
M. D.
, “
The Use of a Microwave Oven for the Rapid Determination of Moisture Content of Soils
,” Road Research Laboratory Report,
Crowthorne, England
, LR280, 15 p.,
1969
.
140.
Hesek
,
J. A.
, and
Wilson
,
R. C.
, “
Use of a Microwave Oven in In-Process Control
,”
Anal. Chem.
, Vol.
46
,
1974
, pp. 1160.
141.
Koh
,
T. S.
, “
Microwave Drying of Biological Tissue for Trace Element Determination
,”
Anal. Chem.
, Vol.
52
,
1980
, pp. 1978–1979.
142.
Doughty
,
D. A.
, “
Determination of Water in Oil Emulsions by a Microwave Resonance Procedure
,”
Anal. Chem.
, Vol.
49
,
1977
, pp. 690–694.
143.
Hasek
,
J. A.
, and
Wilson
,
R. C.
,, “
Practical Analysis of High-Purity Chemicals. X. Use of a Microwave Oven in In-Process Control
,”
Anal. Chem.
, Vol.
46
,
1974
, pp. 1160.
144.
Nadkarni
,
R. A.
,
Botto
,
R. I.
, and
Smith
,
S. E.
, “
Comparison of Two Atomic Spectroscopic Methods for Elemental Analysis of Geological Materials
,”
Atom. Spect.
, Vol.
3
,
1982
, pp. 180–184.
145.
Singhal
,
G. H.
, and
Nadkarni
,
R. A.
, “
Recovery of Catalyst from Coal Liquefaction Residues
,” U. S. Patent 4,434,043,
1984
.
146.
Nadkarni
,
R. A.
, and
Morrison
,
G. H.
, “
Multielemental Instrumental Neutron Activation Analysis of Biological Materials
,”
Anal. Chem.
, Vol.
45
,
1973
, pp. 1957–1960.
147.
Dybczynski
,
J. W.
, and
Suschny
,
O.
, IAEA/RL/64,
1979
.
148.
Nadkarni
,
R. A.
, and
Morrison
,
G. H.
, “
Multielement Analysis of Lake Sediments by Neutron Activation Analysis
,”
Anal. Chim. Acta
, Vol.
99
,
1978
, pp. 133–141.
149.
Fernandez
,
F. J.
, “
Atomic Absorption Determination of Gaseous Hybrids Utilizing Sodium Borohydride Reduction
,”
Atom. Ab. News.
, Vol.
12
,
1973
, pp. 93–97.
150.
Brodie
,
K. G.
, “
A Comparative Study, Determining Arsenic and Selenium by AAS
,” Amer. Lab.,
1977
, pp. 3–78.
151.
Sharkey
,
A. G.
, Jr.,
Kesseler
,
T.
, and
Friedel
,
R. A.
, “
Trace Elements in Coal Dust by Spark Source Mass Spectrometry
,” in
Trace Elements in Fuel
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series, No. 141,
American Chemistry Society
,
Washington, DC
,
1975
, pp. 48–56.
Google Scholar
Crossref
Search ADS
 
152.
Kuhn
,
J. K.
,
Harfst
,
W. F.
, and
Shimp
,
N. F.
, “
X-Ray Fluorescence Analysis of Whole Coal
,” in
Trace Elements in Fuels
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series No. 141,
American Chemical Society
,
Washington, DC
,
1975
, pp. 66–73.
Google Scholar
Crossref
Search ADS
 
153.
Johnson
,
R. G.
,
Sellers
 
G. A.
, and
Fleming
,
S. L.
, II, “
The Determination of Major and Minor Elements in Coal Ash and of Chlorine and Phosphorus in Whole Coal by X-Ray Fluorescence Spectrometry
,” in
Methods for Sampling and Inorganic Analysis of Coal
,
Golightly
 
D. W.
 and
Simon
 
F. O.
, Eds.,
USGS Bulletin 1823
,
U.S. Geological Survey, Washington, DC
,
1989
, pp. 35–39.
154.
Skleen
,
C. J.
,
Libby
,
B. J.
, and
Crandell
,
W. B.
, “
Determination of 62 Elements in Eight Argonne Premium Coal Ash Samples by Automated Semiquantitative Direct Current Arc Atomic Emission Spectrography
,” in
The Chemical Analysis of Argonne Premium Coal Samples
,
Palmer
 
C. A.
, Ed.,
USGS Bulletin 2144
,
U.S. Geological Survey, Washington, DC
,
1995
, pp. 7–13.
155.
Nadkarni
,
R. A.
, “
Nuclear Activation Methods for the Characterization of Fossil Fuels
,”
J. Radioanal. Nucl. Chem.
, Vol.
84
,
1984
, pp. 67–87.
156.
Kennedy
,
E. J.
,
Ruch
,
R. R.
,
Gluskoter
,
H. J.
, and
Shimp
,
N. F.
, in
Nuclear Methods in Environmental Research
,
University of Missouri
,
Columbia, MO
, Vol.
1
,
1971
, p. 205.
157.
Rook
,
H. L.
,
Gills
,
T. E.
, and
LaFleur
,
P. D.
,
Anal. Chem.
, Vol.
44
,
1972
, p. 1144.
158.
Weaver
,
J. N.
, and
Von Lehmden
,
D. J.
,
American Chemical Society, Division of Fuel Chemistry
, Preprint 16,
1972
.
159.
Pericos
,
D. C.
, and
Belkas
,
E. P.
, “
Determination of Uranium M Uraniferous Coal
,”
Talanta
, Vol.
16
,
1969
, pp. 745–748.
160.
Volborth
,
A.
, in
Analytical Methods for Coal and Coal Products
, Vol.
3
,
Karr
 
C.
, Ed.,
Academic Press
,
New York
,
1979
, p. 303.
161.
Block
,
C.
, and
Dams
,
R.
,
Anal. Chim. Acta
, Vol.
68
,
1973
, p. 11.
162.
Block
,
C.
, and
Dams
,
R.
,
Environ. Sci. Technol.
, Vol.
9
,
1975
, p. 146.
163.
Tamura
,
N.
,
Radiochem. Radioanal. Lett.
, Vol.
18
,
1974
, p. 135.
164.
Obrusnik
,
I.
,
Starkova
,
J.
, and
Blazek
,
J.
,
J. Radioanal. Nucl. Chem.
, Vol.
31
,
1976
, p. 495.
165.
Chattopadhyay
,
A.
, and
Jervis
,
R. E.
,
Anal. Chem.
, Vol.
46
,
1974
, p. 219.
166.
Palmer
,
C. A.
, “
Determination of 29 Elements in Eight Argonne Premium Coal Samples by Instrumental Neutron Activation Analysis
,” in
The Chemical Analysis of Argonne Premium Coal Samples
,
Palmer
 
C. A.
, Ed.,
USGS Bulletin 2144
,
U.S. Geological Survey, Washington, DC
,
1995
. pp. 25–32.
167.
Ruch
,
R. R.
,
Cahill
,
R. A.
,
Frost
,
J. K.
,
Camp
,
L. R.
, and
Gluskoter
,
H. J.
,
J. Radioanal. Nucl. Chem.
, Vol.
38
,
1977
, pp. 415–424.
168.
Sheibly
,
D. W.
, “
Trace Elements by Instrumental Neutron Activation Analysis for Pollution Monitoring
,” in
Trace Elements in Fuels
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series No. 141,
American Chemical Society
,
Washington, DC
,
1975
, pp. 98–117.
Google Scholar
Crossref
Search ADS
 
169.
Gluskoter
,
H. J.
, and
Ruch
,
R. R.
,
Fuel
, Vol.
50
,
1971
, p. 65.
170.
Hannan
,
A. H. M. A.
,
Kehinde
,
L. O.
,
Oluwole
,
A. F.
,
Borishade
,
A. B.
,
Oshin
,
O.
,
Aladekomo
,
J. B.
, and
Jervis
,
R. E.
,
Radiochem. Radioanal. Lett.
, Vol.
53
,
1982
, p. 155.
171.
Ayanvglu
,
S. F.
, and
Gunduz
,
G.
,
J. Radioanal. Nucl. Chem.
, Vol.
43
,
1978
, pp. 155–165.
172.
Nadkarni
,
R. A.
, “
Multielement Analysis of Coal and Fly Ash Standards by Instrumental Neutron Activation Analysis
,”
Radiochem. Radioanal. Lett.
, Vol.
21
,
1975
, pp. 161–176.
173.
Abel
,
K. H.
, and
Rancitelli
,
L. A.
, in
Trace Elements in Fuels
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series No. 141,
American Chemical Society
,
Washington, DC
,
1975
, p. 118.
174.
Bolton
,
N. E.
,
Carter
,
J. A.
,
Emery
,
J. F.
,
Feldman
,
C.
,
Fulkerson
,
W
,
Hulett
,
L. D.
, and
Lyon
,
W. S.
, in
Trace Elements in Fuels
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series No. 141,
American Chemical Society
,
Washington, DC
,
1975
, p. 175.
175.
Ragaini
,
R. C.
, and
Ondov
,
J. M.
,
J. Radioanal. Nucl. Chem.
, Vol.
37
,
1977
, p. 679.
176.
Ondov
,
J. M.
,
Zoller
,
W. H.
,
Olmez
,
I.
,
Aras
,
N. K.
,
Gordon
,
G. E.
,
Rancitelli
,
L. A.
,
Abel
,
K. H.
,
Filby
,
R. H.
,
Shah
,
K. R.
, and
Ragaini
,
R. C.
,
Anal. Chem.
, Vol.
47
,
1975
, p. 1102.
177.
Germani
,
M. S.
,
Gokmen
,
I.
,
Sigleo
,
A. C.
, Kowaiczyk,
Olmez
,
I.
,
Small
,
A. M.
,
Anderson
,
D. L.
,
Failey
,
M. P.
,
Gulovali
,
M. C.
,
Choquette
,
C. E.
,
Lepel
,
E. A.
,
Gordon
,
G. E.
, and
Zoller
,
W. H.
,
Anal. Chem.
, Vol.
52
,
1980
, p. 24-.
178.
Filby
,
R. H.
,
Sandstrom
,
D. R.
,
Lytle
,
F. W.
,
Greegor
,
R. B.
,
Khalil
,
S. R.
,
Ekambaram,
,
V.
,
Weiss
,
C. S.
, and
Grimm
,
C. A.
,
NBS Special Publication
, Vol.
618
,
1981
, p. 21.
179.
Carpenter
,
B. S.
, and
Filby
,
R. H.
, in
Atomic and Nuclear Methods in Fossil Energy Research
,
Filby
 
R. H.
, Ed.,
Plenum Press
,
New York
,
1982
, p. 83.
180.
Cahill
,
R. A.
,
Frost
,
J. K.
,
Camp
,
L. R.
, and
Ruch
,
R. R.
, in
Atomic and Nuclear Methods in Fossil Energy Research
,
Filby
 
R. H.
, Ed.,
Plenum Press
,
New York
,
1982
, p. 155.
181.
Garcia
,
S. R.
,
Hensley
,
W. K.
,
Minor
,
M. M.
,
Denton
,
M. M.
, and
Fuka
,
M. A.
, in
Atomic and Nuclear Methods in Fossil Energy Research
,
Filby
 
R. H.
, Ed.,
Plenum Press
,
New York
,
1982
, p. 133.
182.
Al-Shahristani
,
H.
 and
Al-Atyia
,
M. J.
,
J. Radioanal. Nucl. Chem.
, Vol.
14
,
1973
, p. 401.
183.
Chen
,
S. G.
,
Tsai
,
H. T.
, and
Wu
,
S. C.
,
Radiochem. Radioanal. Lett
., Vol.
49
,
1981
, p. 149.
184.
Frost
,
J. K.
,
Koszykowski
,
R. F.
, and
Klemm
,
R. C.
,
J. Radioanal. Nucl. Chem.
, Vol.
71
,
1982
, p. 199.
185.
Fruchter
,
J. S.
,
Laul
,
J. C.
,
Petersen
,
M. R.
,
Ryan
,
P. W.
, and
Turner
,
M. E.
,
Advances in Chemistry
Series No. 170,
American Chemical Society
,
Washington, DC
,
1978
, p. 255.
186.
Fox
,
J. P.
,
Evans
,
J. C.
,
Wildman
,
T. R.
, and
Fruchter
,
J. S.
, LBL-890-1,
1979
.
187.
Fox
,
J. P.
,
Mason
,
K. K.
, and
Duvall
,
J. J.
, LBL-9030,
1979
.
188.
Shendriker
,
A. D.
 and
Faudel
,
G. B.
,
Environ. Sci. Technol.
, Vol.
12
,
1978
, p. 332.
189.
Fruchter
,
J. S.
,
Wilkerson
,
C. L.
,
Evans
,
J. C.
, and
Sanders
,
R. W.
, in
Atomic and Nuclear Methods in Fossil Energy Research
,
Filby
 
R. H.
, Ed.,
Plenum Press
,
New York
,
1982
, p. 155.
190.
Jacobs
,
F. S.
, and
Filby
,
R. H.
,
Anal. Chem.
, Vol.
55
,
1983
, p. 74.
191.
Jervis
,
R. E.
,
Ho
,
K. L. R.
, and
Tiefenbach
,
B.
,
J. Radioanal. Nucl. Chem
., Vol.
71
, p. 225.
192.
Jacobs
,
F. S.
, and
Filby
,
R. H.
, in
Atomic and Nuclear Methods in Fossil Energy Research
,
Filby
 
R. H.
, Ed.,
Plenum Press
,
New York
,
1982
, p. 49.
193.
Shah
,
K. R.
,
Filby
,
R. H.
, and
Haller
,
W. A.
,
J. Radioanal. Nucl. Chem.
, Vol.
6
,
1970
, pp. 185, 413.
194.
Persiani
,
C.
 and
Shelby
,
W. D.
,
Environ. Sci. Technol.
, Vol.
7
,
1973
, p. 125.
195.
Filby
,
R. H.
,
Shah
,
K. R.
, and
Yaghmaie
,
F.
 in
Ash Deposits and Corrosion Due to Impurities in Combustion Gases
,
Bryers
 
R. W.
, Ed.,
McGraw Hill
,
New York
,
1978
, p. 51.
196.
Guinn
,
V. P.
,
Bryan
,
D. E.
, and
Lukens
,
H. R.
, in
Nuclear Techniques in Environmental Pollution
,
IAEA
,
Vienna, Austria
,
1971
, p. 347.
197.
Siemer
,
D. D.
,
Koteel
,
P.
, and
Jariwala
,
V.
,
J. Radioanal. Nucl. Chem.
, Vol.
48
,
1976
, pp. 836–840.
198.
Filby
,
R. H.
, and
Shah
,
K. R.
, in
Nuclear Methods in Environmental Research
, Vol.
1
,
1971
, p. 86.
199.
Lukens
,
H. R.
,
Bryan
,
D.
,
Hiatt
,
N. A.
, and
Schlensinger
,
H. L.
, Gulf-RT-A-10684,
1971
.
200.
Lukens
,
H. R.
, Gulf-RT-A10973,
1972
.
201.
Filby
,
R. H.
,
Shah
,
K. R.
, and
Sautter
,
C. A.
,
J. Radioanal. Nucl. Chem.
, Vol.
37
, p. 693.
202.
Augenstein
,
S.
, “
New Ruling on Power Plants a Breath of Fresh Air for New Jersey
,” New Jersey Star Ledger, December 22,
2011
.
203.
Bate
,
L. C.
,
Radiochem. Radioanal. Lett.
, Vol.
6
,
1971
, p. 139.
204.
McFarland
,
R. C.
,
Radiochem. Radioanal. Letters
, Vol.
16
,
1973
, p. 47.
205.
Weiss
,
H. V.
 and
Chew
,
K.
,
Anal. Chim. Acta
, Vol.
67
,
1973
, p. 444.
206.
Moody
,
J. R.
,
Paulsen
,
P. J.
,
Rains
,
T. C.
, and
Rook
,
H. L.
, in Accuracy in Trace Analysis, NBS Special Publication No. 422,
1976
, p. 267.
207.
Feldman
,
C.
,
Anal. Chem.
, Vol.
46
,
1974
, p. 99.
208.
Lo
,
J. M.
 and
Wai
,
C. M.
,
Anal. Chem.
, Vol.
47
,
1975
, p. 1869.
209.
Sanemasa
,
I.
,
Deguchi
,
T.
,
Urata
,
K.
,
Tomooka
,
J.
, and
Nagai
,
H.
,
Anal. Chim. Acta
, Vol.
87
,
1976
, p. 479.
210.
Toribara
,
T. Y.
,
Shields
,
C. P.
, and
Koval
,
L.
,
Talanta
, Vol.
17
,
1970
, p. 1025.
211.
Weiss
,
H. V.
,
Shipman
,
W. H.
, and
Guttman
,
M. A.
,
Anal. Chim. Acta
, Vol.
81
,
1976
, p. 211.
212.
Carron
,
J.
, and
Agemian
,
H.
,
Anal. Chim. Acta.
, Vol.
92
,
1977
, p. 61.
213.
Hatch
,
W. R.
, and
Ott
,
W. L.
,
Anal. Chem.
, Vol.
40
,
1968
, p. 2085.
214.
Long
,
S. E.
, and
Kelly
 
W. R.
, “
Determination of Mercury in Coal by Isotope Dilution Cold-Vapor Generation Inductively Coupled Plasma Mass Spectrometry
,”
Anal. Chem.
, Vol.
74
,
2002
, pp. 1477–1483.
215.
Magee
,
E. M.
,
Hall
,
H. J.
, and
Varga
, ,
G. M.
 Jr., EPA-R2-73-249,
1973
.
216.
Zubovic
,
P.
, EPA-600/2-76-149,
1976
.
217.
Bonnett
,
R.
, and
Czechowski
,
F.
,
Nature
, Vol.
283
,
1980
, p. 465.
218.
Wewerka
,
E. M.
,
Williams
,
J. M.
,
Vanderborgh
,
N. E.
,
Harman
,
A. W.
,
Wagner
,
P.
 
Wanek
,
P. L.
, and
Olsen
,
J. D.
, EPA-600/7-78-028a,
1978
.
219.
Watling
,
R. J.
,
Watling
,
H. R.
, and
Wardale
,
I. M.
,
Symp. Anal. Chem. Exploration, Mining, and Processing Materials
,
Johannesburg
, 156,
1976
.
220.
Waters
,
R. F.
, and
Kenworthy
,
H.
,
U.S. Bureau of Mines
, RI-6940,
1967
.
221.
Swaine
,
D. J.
, in
Symposium of Trace Substances in Environmental Health
,
Columbia, MO
, XI, 107,
1977
.
222.
Smith
,
R. D.
,
Campbell
,
J. A.
, and
Nielson
,
K. K.
,
Environ. Sci. Technol.
, Vol.
13
,
1979
, p. 553.
223.
Somerville
,
M. H.
, and
Elder
,
J. L.
, University of North Dakota Bulletin 77-09-EES-01,
1977
.
224.
Weeks
,
R. A.
, in U.S. Mineral Resources,
Brobst
 
D. A.
 and
Pratt
 
W. P.
, Eds. U.S. Geological Survey Professional Paper, 820, 237,
1973
.
225.
Sandell
,
E. B.
,
Colorimetric Determination of Traces of Metals
, 3rd ed.,
Interscience Publishers
,
New York
,
1959
.
226.
Jankovsky
,
J.
,
Talanta
, Vol.
2
,
1959
, p. 99.
227.
Nadkarni
,
R. A.
,
Tejam
,
B. M.
, and
Haldar
,
B. C.
, “
Determination of Gallium in Rocks by Neutron Activation Analysis and Substoichiometric Extraction with Malachite Green
,”
Radiochem. Radioanal. Lett.
, Vol.
12
,
1972
, pp. 235–244.
228.
Wangell
,
L. E.
, and
Gladney
,
E. S.
,
Anal. Chim. Acta
, Vol.
96
,
1978
, p. 271.
229.
Giauque
,
R. D.
,
Garrett
,
R. B.
, and
Goda
,
L. Y.
,
Anal. Chem.
, Vol.
49
,
1977
, p. 1012.
230.
Rowe
,
J. J.
, and
Steinnes
,
E.
, in Modern Trends in Activation Analysis, Munich, 1, 529,
1976
.
231.
Klein
,
D. H.
,
Andren
,
A. W.
,
Carter
,
J. A.
,
Emery
,
J. F.
,
Feldman
,
C.
,
Fulkerson
,
W.
,
Lyon
,
W. S.
,
Ogle
,
J. C.
,
Talmi
,
Y.
,
Van Hook
,
R. I.
, and
Bolton
,
N.
,
Environ. Sci. Technol.
, Vol.
9
,
1975
, p. 973.
232.
Owens
,
J. W.
, and
Gladney
,
E. S.
,
Atomic Abs. News.
, Vol.
15
,
1976
, p. 95.
233.
Hancock
,
R. G. V.
,
Anal. Chem.
, Vol.
48
,
1976
, p. 1443.
234.
Sims
,
P. C.
, Preprint,
Purdue University Accelerator Laboratory
,
1978
.
235.
Giauque
,
R. D.
,
Garrett
,
R. B.
, and
Goda
,
L. Y.
,
Anal. Chem.
, Vol.
51
,
1979
, p. 511.
236.
Nadkarni
,
R. A.
, and
Botto
,
R. I.
, “
Determination of Germanium in Coal Ashes by Inductively Coupled Plasma Atomic Emission Spectroscopy
,”
Applied Spec.
, Vol.
38
,
1984
, pp. 595–598.
237.
Musgrave
,
J. R.
, in
Treatise on Analytical Chemistry
,
Kolthoff
 
I. M.
,
Elving
 
P. J.
, and
Sandell
 
E. B.
, Eds.,
Interscience Publishers
,
New York
,
1962
, Part 2, Vol.
2
, p. 297.
238.
Waring
,
C. L.
, and
Tucker
,
W. P.
,
Anal. Chem.
, Vol.
26
,
1954
, p. 1198.
239.
Boumans
,
P. W. J. M.
,
Line Coincidence Tables for Inductively Coupled Plasma Atomic Emission Spectrometry
,
Pergamon Press Ltd.
,
Oxford, New York
,
1980
.
240.
Pollock
,
E. N.
, in
Trace Elements in Fuels
,
Babu
 
S. P.
, Ed.,
Advances in Chemistry
Series No. 141,
American Chemical Society
,
Washington, DC
,
1975
, p. 23.
241.
Waring
,
C. L.
, and
Tucker
,
W. P.
,
Anal. Chem.
, Vol.
26
,
1954
, p. 1198.
242.
Cooley
,
W. E.
,
J. Chem. Educ.
, Vol.
47
,
1970
, p. 177.
243.
Frant
,
M. S.
, and
Ross
,
J. W.
,
Science
, Vol.
154
,
1966
, p. 1553.
244.
Crossley
,
H. E.
,
J. Soc. Chem. Ind.
, Vol.
63
,
1944
, pp. 280–289, 342.
245.
Thomas
, ,
J.
 Jr. and
Gluskoter
,
H. J.
, “
Determination of Fluoride in Coal with the Fluoride Ion Specific Electrode
,”
Anal. Chem.
, Vol.
46
,
1974
, pp. 1321–1323.
246.
Conrad
,
V. B.
, and
Brownlee
,
W. D.
, “
Hydropyrolytic Ion Chromatographic Determination of Fluoride in Coal and Geological Materials
,”
Anal. Chem.
, Vol.
60
,
1988
, pp. 365–369.
247.
Nadkarni
,
R. A.
, and
Pond
,
D. M.
, “
Applications of Ion Chromatography for Determination of Selected Elements in Coal and Oil Shale
,”
Anal. Chim. Acta
, Vol.
146
, pp. 261–266.
248.
Nadkarni
,
R. A.
, “
Applications of Hydride Generation Atomic Absorption Spectrometry for Coal Analysis
,”
Anal. Chim. Acta
, Vol.
135
,
1982
, pp. 363–368.
249.
Robbins
,
W. B.
, and
Caruso
,
J. A.
,
Anal. Chem.
, Vol.
51
,
1979
, p. 889A.
250.
Fleming
,
H. D.
, and
Ide
,
R. G.
,
Anal. Chim. Acta
, Vol.
83
,
1976
, pp. 67–82.
251.
Godden
,
R. G.
, and
Thomerson
,
D. R.
,
Analyst
, Vol.
105
,
1980
, p. 1137.
252.
Brodie
,
K. G.
,
Amer. Lab.
, Vol.
11
,
1979
, pp. 58–66; and Vol.
9
,
1977
pp. 73–79.
253.
Botto
,
R. I.
, “
Multielement Analysis of Fossil Fuels and Related Materials by ICP-AES
,” Spectrochim. Acta Reviews, 14, 141-159,
1991
.
254.
Kang
,
H. K.
, and
Valentile
,
J. L.
,
Anal. Chem.
, Vol.
49
,
1977
, pp. 1829–1832.
255.
Pierce
,
F. D.
, and
Brown
,
H. R.
,
Anal. Chem.
, Vol.
48
,
1976
, pp. 693–695; and Vol.
49
,
1977
, pp. 1417–1422.
256.
Smith
,
A. E.
,
Analyst
, Vol.
100
,
1975
, pp. 300–306.
257.
Knudson
,
E. J.
, and
Christian
,
G. D.
,
Atom. Abs. News.
, Vol.
13
,
1974
, p. 74.
258.
Fernandez
,
F. J.
, and
Manning
,
D. C.
,
Atom. Abs. News.
, Vol.
10
,
1971
, p. 86.
259.
Fiorino
,
J. A.
,
Jones
,
J. W.
, and
Capar
,
S. G.
,
Anal. Chem.
, Vol.
48
,
1976
, pp. 120–125.
260.
Chapman
,
J. F.
, and
Dale
,
L. S.
,
Anal. Chem.
, Vol.
111
,
1979
, pp. 137–144.
261.
Freeman
,
H. C.
, and
Uthe
,
J. F.
,
Atom. Abs. News.
, Vol.
13
,
1974
, p. 75.
262.
Lansford
,
M.
,
McPherson
,
E. M.
, and
Fishman
,
M. J.
,
Atom. Abs. News
, Vol.
13
, p. 103.
263.
Fernandez
,
F. J.
,
Atom. Abs. News
, Vol.
12
,
1973
, p. 93.
264.
Manning
,
D. C.
,
Atom. Abs. News
, Vol.
10
,
1971
, p. 123.
265.
Pierce
,
F. D.
,
Lamoreaux
,
J. C.
,
Brown
,
H. R.
, and
Fraser
,
R. S.
,
Appl. Spectrosc.
, Vol.
30
,
1976
, p. 38.
266.
Nakashima
,
S.
,
Anal. Chem.
, Vol.
51
,
1979
, pp. 654–656.
267.
Pyen
,
G.
, and
Fishman
,
M.
,
Atom. Abs. News.
, Vol.
17
,
1978
, pp. 47–48.
268.
Kirkbright
,
G. F.
, and
Taddia
,
M.
,
Atom. Abs. News.
, Vol.
18
,
1979
, pp. 68–70.
269.
Vijan
,
P. N.
,
Amer. Lab.
, Vol.
11
,
1979
, pp. 32–43.
270.
Chan
,
C. Y.
, and
Vijan
,
P. N.
,
Anal. Chim. Acta
, Vol.
101
,
1978
, p. 33.
271.
Nakashima
,
S.
,
Anal. Chim. Acta
, Vol.
105
,
1980
, pp. 732–733.
272.
Vijan
,
P. N.
, and
Chan
,
C. Y.
,
Anal. Chem.
, Vol.
48
,
1976
, pp. 1788–1792.
273.
Subramanian
,
K. S.
, and
Sastri
,
V. S.
,
Talanta
, Vol.
27
,
1980
, pp. 469–472.
274.
Evans
,
W. H.
,
Jackson
,
F. J.
, and
Deller
,
D.
,
Talanta
, Vol.
104
,
1979
, pp. 16–34.
275.
Hodge
,
V. F.
,
Seidel
,
S. L.
, and
Goldberg
,
E. D.
,
Talanta
, Vol.
51
,
1979
, pp. 1256–1259.
276.
Hahn
,
M. H.
,
Mulligan
,
K. J.
,
Jackson
,
M. E.
, and
Caruso
,
J. A.
,
Anal. Chim. Acta
, Vol.
118
,
1980
, pp. 115–122.
277.
Vijan
,
P. N.
, and
Wood
,
G. R.
,
Analyst
, Vol.
101
,
1976
, p. 966.
278.
Vijan
,
P. N.
, and
Sadana
,
R. S.
,
Talanta
, Vol.
27
,
1980
, pp. 321–326.
279.
Thompson
,
K. C.
,
Analyst
, Vol.
100
,
1975
, p. 307.
280.
Chattopadhyay
,
A.
, and
Jervis
,
R. E.
,
Anal. Chem.
, Vol.
46
,
1974
, p. 1630.
281.
Gladney
,
E. S.
, and
Rook
,
H. L.
,
Anal. Chem.
, Vol.
47
,
1975
, p. 1554.
282.
Pollock
,
E. N.
, and
West
,
S. J.
,
Atom. Abs. News.
, Vol.
12
,
1973
, p. 6.
283.
Thompson
,
M.
, and
Phlavanpour
,
B.
,
Anal. Chim. Acta
, Vol.
109
,
1979
, pp. 251–258.
284.
Nadkarni
,
R. A.
, “
Determination of Volatile Elements in Coal and Other Organic Materials by Oxygen Bomb Combustion
,”
Amer. Lab.
, Vol.
13
,
1981
, pp. 22–29.
285.
Shannon
,
D. G.
, and
Fine
,
L. O.
,
Environ. Sci. Technol.
, Vol.
8
,
1974
, p. 1026.
286.
Green
,
J. B.
, and
Manahan
,
S. E.
,
Anal. Chem.
, Vol.
50
,
1978
, p. 1975.
287.
Somerville
,
M. H.
, and
Elder
,
J. L.
, University of North Dakota Bulletin 77-09-EES-01,
1977
.
288.
Churey
,
D. L.
,
Gutenmann
,
W. H.
,
Pendias
,
A. K.
, and
Lisk
,
D. J.
,
J. Agri. Food Chem.
, Vol.
27
,
1979
, p. 910.
289.
Williams
,
J. M.
,
Wewerka
,
E. M.
,
Vanderborgh
,
N. E.
,
Wagner
,
P.
,
Wanek
,
P. L.
, and
Olsen
,
J. D.
, LA-UR-77-1850.
290.
Dressen
,
D. R.
,
Wangner
,
L. E.
,
Gladney
,
E. S.
, and
Owens
,
J. W.
,
Proceedings of the Symposium on Environmental Chemistry and Cycling Processes
,
Augusta, GA
, p. 140.
291.
James
,
W. D.
,
Janghorbani
,
M.
, and
Baxter
,
T.
,
Anal. Chem.
, Vol.
49
,
1977
, p. 1994.
292.
Cox
 
J. A.
,
Lundquist
,
G. L.
,
Przyjany
,
A.
, and
Schmulbach
,
C. D.
,
Environ. Sci. Technol.
, Vol.
12
,
1978
, p. 722.
293.
Halligan
,
A. S.
, and
Pagenkopf
,
G. K.
,
Environ. Sci. Technol.
, Vol.
14
,
1980
, p. 995.
294.
Fisher
,
G. L.
,
Silberman
,
D.
,
Prentice
,
B. A.
,
Heft
,
R. E.
, and
Ondov
,
J. M.
,
Environ. Sci. Technol.
, Vol.
13
,
1979
, pp. 689.
295.
Phung
,
H. T.
,
Lund
,
L. J.
,
Page
,
A. L.
, and
Bradford
,
G. R.
,
J. Environ. Qual
., Vol.
8
, p. 171.
296.
Nichols
,
D. G.
,
Servais
,
R. A.
, and
Rolinski
,
E. J.
, CONF-790571-1,
1979
.
297.
Schuller
,
R. M.
,
Suloway
,
J. J.
,
Griffin
,
R. A.
,
Rissell
,
S. J.
, and
Childers
,
W. F.
, Society of Mineral Engineers, Minisymposium Series 79-06, New Orleans, LA,
1979
, p. 7.
298.
Guthrie
,
R. K.
, and
Cherry
,
D. S.
,
Water Res. Bull.
, Vol.
15
,
1979
, p. 244.
299.
Theis
,
T. L.
, and
Richter
,
R. O.
,
Environ. Sci. Technol.
, Vol.
13
,
1979
, p. 219.
300.
Tessier
,
A.
,
Campbell
,
P. G. C.
, and
Bisson
,
M.
,
Anal. Chem.
, Vol.
51
,
1979
, p. 844.
301.
McBride
,
J. P.
,
Moore
,
R. E.
,
Witherspoon
,
J. P.
, and
Blanco
,
R. E.
,
Science
, Vol.
202
,
1978
, p. 1045.
302.
Alderman
,
J. K.
,
Grady
,
W. C.
,
Simonyi
,
T.
, and Simcoe, Coal Research Bureau, University of West Virginia, 160,
1978
.
303.
Papastefanou
,
C.
 and
Charalambous
,
S.
,
Z. Naturforsch
, Vol.
34A
,
1979
, p. 533.
304.
Coles
,
D. C.
,
Ragaini
,
R. C.
, and
Ondov
,
J. M.
,
Environ. Sci. Technol.
, Vol.
12
,
1978
, p. 442.
305.
Eisenbud
,
M.
, and
Petrow
,
H. G.
,
Science
, Vol.
144
,
1964
, p. 288.
306.
Martin
,
J. E.
,
Harward
,
E. D.
, and
Oakley
,
D. T.
, Bur. Radiol. Health, Appendix 14, November
1969
.
307.
Hull
,
A. P.
,
Nucl. Safety
, Vol.
12
,
1971
, p. 185.
308.
Terrell
,
J. G.
,
Harward
,
E. D.
, and
Leggett
,
I.
,
Ind. Med. Surgery
, Vol.
36
,
1967
, p. 412.
309.
Mishra
,
U. C.
,
Lalit
,
B. Y.
, and
Ramachandran
,
T. V.
,
Sci. Total Environ.
, Vol.
14
, p. 77.
310.
Barber
,
D. E.
, and
Giorgio
,
H. R.
,
Health Phys.
, Vol.
32
,
1977
, p. 83.
311.
Christiansen
,
C. S.
,
Ledbetter
,
J. O.
, and
Miksad
,
R. W.
,
Proceedings of the Annual Meeting of the Air Pollution Control Association
, 72nd, (2), 19.5,
1979
.
312.
Krieger
,
H.
, and
Jacobs
,
B.
, EPA-600/4-78-039,
1978
.
313.
Koester
,
P. A.
, and
Zieger
,
W. H.
, EPA-600/7-78-185,
1978
.
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