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ASTM Selected Technical Papers
Chemical and Biological Characterization of Municipal Sludges, Sediments, Dredge Spoils, and Drilling Muds
By
JJ Lichtenberg
JJ Lichtenberg
1
U.S. Environmental Protection Agency
,
Cincinnati, OH 45268
;
symposium chairman and editor
.
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JA Winter
JA Winter
editor
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CI Weber
CI Weber
editor
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L Fradkin
L Fradkin
editor
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ISBN-10:
0-8031-0987-3
ISBN:
978-0-8031-0987-2
No. of Pages:
520
Publisher:
ASTM International
Publication date:
1988

This paper describes a user-friendly IBM-PC compatible computer program capable of managing the Quality Assurance/Quality Control (QA/QC) requirements of any size laboratory performing analysis to Environmental Protection Agency (EPA) specifications. The program design criteria addresses the QA/QC requirements of the analysis of sludges, sediments, waters, and other materials. The database is initialized using well established standard data for solids and liquids (for example, Standard Reference Materials from the National Bureau of Standards). The analyst enters the following QC data for the parameters of interest into the database: found concentrations for internal and/or external standards, values for blanks, spike recoveries, replicates, duplicates, and midpoint internal standards. This step is performed for each parameter for each discrete sample set or analytical run. The program then generates control charts for these parameters and creates a QC data sheet, which documents all aspects of the QA/QC requirements for chemical analysis as specified by the EPA. This database management system also transfers the QA/QC documentation into a universal format capable of being used in standard statistical and spreadsheet software, such as Lotus 1-2-3, Supercalc 4, Chartmaster, and others. This allows a wide range of statistical and graphical manipulations to be performed not only on the QA/QC data but on the analytical data as well.

1.
Methods for Chemical Analysis of Water and Wastes
,” EPA-600/4-79-020,
U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory
,
Cincinnati, OH
,
1979
.
2.
Standard Methods for the Examination of Water and Wastewater
,”
American Public Health Association
,
Washington, DC
,
1985
, 1268 pp.
3.
Section 11—Water and Environmental Technology
,”
American Society for Testing and Materials
,
Philadelphia
,
1985
, Volume
11.01
, Water (I), 640 pp.
4.
Handbook for Analytical Quality Control in Water and Wastewater Laboratories
,” EPA-600/4-79-019,
U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory
,
Cincinnati, OH
,
1979
.
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