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ASTM Selected Technical Papers
Fractography of Modern Engineering Materials: Composites and Metals
By
JE Masters
JE Masters
1
Senior Research Engineer
,
American Cyanamid Co.
,
Stamford, CT 06904
;
symposium cochairman and coeditor
.
Search for other works by this author on:
JJ Au
JJ Au
2
Sundstrand Corp.
,
editor
Search for other works by this author on:
ISBN-10:
0-8031-0950-4
ISBN:
978-0-8031-0950-6
No. of Pages:
470
Publisher:
ASTM International
Publication date:
1987

A combination of macroscopic delamination fracture toughness, scanning electron microscope (SEM) real-time fracture observations, and postfracture morphology were used to study the micromechanical processes of delamination failure in several graphite/epoxy systems.

Strain energy release rate GIc, GIIc, and mixed mode GI&IIc were obtained from unidirectional double cantilever beam specimens. Comparisons of these energy release rates with the resulting fracture surface mophology are used to clarify the relative importance of the formation of hackles and the fiber matrix interface adhesion to delamination toughness under Mode I, Mode II, and mixed Mode I & II loading conditions.

Real-time fracture observations of composite delamination in the SEM revealed the microprocesses of microcrack formation and coalescence. These observations coupled with GIc for the neat material, determined from compact tension specimens, provide insight on how resin toughness can be translated into composite delamination toughness.

The implications of hackle formation and their importance in the failure analysis of graphite/epoxy systems are discussed.

1.
Hunston
,
D. L.
and
Bullman
,
G. W.
, “
Characterization of Interlaminar Crack Growth in Composites: Double Cantilever Beam Studies
,” in
1985 Grant and Contract Review
, Vol.
II
,
NASA Langley Research Center Materials Division
,
Fatigue and Fracture Branch
, 13–14 Feb. 1985.
2.
Chakachery
,
E. A.
and
Bradley
,
W. L.
, “
A Comparison of the Crack Tip Damage Zone for Fracture of Hexcel F185 Neat Resin and T6T145/F185 Composite
,” presented at the
ACS International Symposium on Non-Linear Deformation, Fatigue and Fracture of Polymeric Materials
,
Chicago, IL
, 8–13 Sept. 1985,
American Chemical Society
,
Washington, DC
.
3.
Morris
,
G. E.
, “
Determining Fracture Directions and Fracture Origins on Failed Graphite/Epoxy Surfaces
,” in
Nondestructive Evaluation and Flaw Criticality for Composite Materials
, ASTM STP 696,
American Society for Testing and Materials
,
Philadelphia
1979
, pp. 274-297.
4.
Tse
,
M. K.
,
Hibbs
,
M. F.
, and
Bradley
,
W. L.
, “
Interlaminar Fracture Toughness and Real-Time Fracture Mechanism of Some Toughened Graphite/Epoxy Deposits
,” presented at the
ASTM Symposium on Toughened Composites
,
Houston, TX
, 13–15 March 1985, in
Toughened Composites
, STP 937,
American Society for Testing and Materials
,
Philadelphia
, 1987.
5.
Devitt
,
D. F.
,
Schapery
,
R. A.
, and
Bradley
,
W. L.
, “
A Method for Determining the Mode I Delamination Fracture Toughness of Elastic and Viscoelastic Composite Materials
,”
Journal of Composite Materials
, Vol.
14
,
10
1980
, pp. 270-285.
6.
Whitney
,
J. M.
,
Browning
,
C. E.
, and
Hoogsteden
,
W.
, “
A Double Cantilever Beam Test for Characterizing Mode I Delamination of Composite Materials
,”
Journal of Reinforced Plastics and Composites
, Vol.
1
,
10
1982
, pp. 297-313
7.
Wilkins
,
D. J.
,
Eisenmann
,
J. R.
,
Cumin
,
R. A.
, and
Margolis
,
W. S.
, “
Characterizing Delamination Growth in Graphite/Epoxy
,” in
Damage in Composite Materials
, ASTM STP 775,
American Society for Testing and Materials
,
Philadelphia
,
1982
, pp. 168-183.
8.
Russell
,
A. J.
and
Street
,
K. N.
, “
Moisture and Temperature Effects on the Mixed-Mode Delamination Fracture of Unidirectional Graphite Epoxy
,” in
Delamination and Debonding of Materials
,
American Society for Testing and Materials
,
Philadelphia
,
1985
.
9.
Bradley
,
W. L.
and
Cohen
,
R. N.
, “
Matrix Deformation and Fracture in Graphite Reinforced Epoxies
,” in
Delamination and Debonding of Materials
, ASTM STP 876,
American Society for Testing and Materials
,
Philadelphia
,
1985
.
10.
Jordan
,
W. M.
, “
The Effect of Resin Toughness on the Delamination Fracture Behavior of Graphite/Epoxy Composites
,” Ph.D. dissertation,
Texas A&M University
, College Station, TX,
1985
.
11.
Bascom
,
W. D.
, “
Fractographic Analysis of Interlaminar Fracture
,” presented at the
ASTM Symposium on Toughened Composites
,
Houston, TX
, 13–15 March 1985, in
Toughened Composites
, STP 937,
American Society for Testing and Materials
,
Philadelphia
, 1987.
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