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ASTM Selected Technical Papers
Practical Applications of Quantitative Metallography
By
JH Steele, Jr Jr
JH Steele, Jr Jr
1
Armco Inc.
,
Middletown, Ohio 45043
;
symposium cochairman and editor
.
Search for other works by this author on:
JL McCall
JL McCall
2
Battelle Columbus Laboratories
,
Columbus, Ohio 43201
;
symposium cochairman and editor
.
Search for other works by this author on:
ISBN-10:
0-8031-0220-8
ISBN:
978-0-8031-0220-0
No. of Pages:
193
Publisher:
ASTM International
Publication date:
1984

Methods used to measure planar grain size, either manually or by image analysis, are reviewed based on their historical development and their relationship to basic stereological concepts. The methods discussed include comparison techniques employing standard charts or the Shepherd fracture grain size standards; measurement techniques based on determination of the number of grains per unit area (Jeffries method), the number of triple points per unit area, or the number of grains intercepted or grain boundaries intersected per unit length of a test line (Heyn method); and correlations based on grain shape assumptions for estimating spatial grain size characteristics. Specific procedures for measuring the grain size of nonequiaxed, duplex, or multiphased grain structures are also discussed. Examples of these techniques are given, along with information about the accuracy of grain size measurements.

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,
M.
and
Grolier
,
J.
,
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111
,
12
1977
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2.
Smith
,
C. S.
, “
Grain Shapes and Other Metallurgical Applications of Topology
,”
Metal Interfaces
,
American Society for Metals
,
Cleveland
,
1952
, pp. 65-113.
3.
Smith
,
C. S.
,
Metallurgical Reviews
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9
,
1964
, pp. 1-48.
4.
Hull
,
F. C.
and
Houk
,
W. J.
,
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, Vol.
197
,
04
1953
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5.
Desch
,
C. H.
,
Journal of the Institute of Metals
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22
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1919
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6.
Williams
,
W. M.
and
Smith
,
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,
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, Vol.
197
,
07
1952
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and
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,
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, Vol.
67
,
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8.
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,
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, No.
1
,
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R. C.
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,”
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,
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10.
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, and
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11.
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12.
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13.
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H. A.
,
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,
R. F.
, and
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, “
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,”
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Berglund
,
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,
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11
,
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),
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,
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16.
ASTM Standard Methods for Estimating the Average Grain Size of Metals
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American Society for Testing and Materials
,
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17.
Brandis
,
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and
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,
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18.
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,
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and
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19.
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,
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,
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20.
Shepherd
,
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,
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, Vol.
22
,
12
1934
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21.
Enlund
,
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,
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134
, No.
11
,
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22.
Grossman
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,
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, Vol.
167
,
1946
, pp. 39-79.
23.
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,
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, Vol.
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,
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24.
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,
Z.
,
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,
A. H.
, and
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E. B.
,
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, Vol.
54
,
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25.
Jeffries
,
Z.
,
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, Vol.
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,
1916
, pp. 40-56.
26.
Heyn
,
E.
,
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, Vol.
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,
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27.
Hilliard
,
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,
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,
05
1964
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28.
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,
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,
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,
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29.
Snyder
,
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and
Graff
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,
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,
04
1938
, pp. 377-380.
30.
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,
H.
and
Wiebking
,
K.
,
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, Vol.
8
, No.
1
,
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, pp. 41-45.
31.
Scheil
,
E.
,
Zeitschrift für Metallkunde
 0044-3093, Vol.
27
,
1935
, pp. 199-209;
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,
E.
and
Wurst
,
H.
,
Zeitschrift für Metallkunde
 0044-3093, Vol.
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,
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32.
Johnson
,
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,
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,
01
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33.
Kostron
,
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,
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, Vol.
3
,
06
1949
, pp. 193-203, and July 1949, pp. 229–242.
34.
Aaron
,
H. B.
,
Smith
,
R. D.
, and
Underwood
,
E. E.
, “
Spatial Grain-Size Distribution from Two-Dimensional Measurements
,”
First International Congress of Stereology
,
Vienna
, 18–20 April, 1963, pp. 16-1 to 16-8.
35.
Saltykov
,
S. A.
, “
The Determination of the Size Distribution of Particles in an Opaque Material from Measurement of the Size Distribution of their Sections
,”
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,
Springer-Verlag
,
New York
,
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36.
Exner
,
H. E.
,
International Metallurgical Reviews
, Vol.
17
,
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37.
Okazaki
,
K.
and
Conrad
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H.
,
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, Vol.
13
,
05
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38.
Bodyako
,
M. N.
,
Kasichev
,
V. P.
, and
Naumovich
,
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,
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, Vol.
17
,
05
1980
, pp. 232-237.
39.
Warren
,
R.
and
Durand
,
M. C.
, “
Computer Synthesis of Microstructures in Stereological Analysis
,”
Swedish Symposium on Non-Metallic Inclusions
,
Sodertalje, Sweden
,
1981
, pp. 269-284.
40.
Rhines
,
F. N.
,
Craig
,
K. R.
, and
Rouse
,
D. A.
,
Metallurgical Transactions
 0026-086X, Vol.
7A
,
11
1976
, pp. 1729-1734.
41.
Patterson
,
B. R.
and
Rhines
,
F. N.
, “
Serial Section Estimate of Number Per Unit Volume
,”
Microstructural Science
, Vol.
7
,
Elsevier North-Holland
,
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,
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, pp. 457-462.
42.
Hilliard
,
J. E.
, “
Grain-Size Estimation
,” Report No. 62-RL-3133M,
General Electric Research Laboratory
, Schenectady, N.Y.,
12
1962
.
43.
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,” Special Report No. 5,
Japanese Society for the Promotion of Science
, Tokyo,
04
11
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.
44.
Schuckher
,
F.
,
Acta Polytechnica Scandinavica
,
1966
, pp. 1-102 (see also Ref , pp. 201–265).
45.
Pereira da Silva
,
P. S. C.
, “
Grain Size Measurement
,” M.S. thesis,
University of Sheffield
, England,
09
1966
.
46.
Gokhale
,
A. M.
,
Transactions of the Indian Institute of Metals
, Vol.
35
,
12
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, pp. 595-600.
47.
Saltykov
,
S. A.
,
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, 2nd ed.,
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,
Moscow
,
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(rough draft translation AD 267–700 and 267–701, Armed Services Technical Information Agency); 3rd ed.,
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.
48.
De Hoff
,
R. T.
and
Rhines
,
F. N.
, Eds.,
Quantitative Microscopy
,
McGraw-Hill
,
New York
,
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.
49.
Underwood
,
E. E.
,
Quantitative Stereology
,
Addison-Wesley
,
Reading, Mass.
,
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.
50.
Fullman
,
R. L.
,
Transactions of the A.I.M.E.
, Vol.
197
,
03
1953
, pp. 447-452.
51.
Miller
,
G. A.
,
Avery
,
D. H.
, and
Backofen
,
W. A.
,
Transactions of the A.I.M.E.
, Vol.
236
,
12
1966
, pp. 1667-1673.
52.
Thompson
,
A. W.
,
Metallography
 0026-0800, Vol.
5
,
1972
, pp. 366-369.
53.
Rutherford
,
J. J. B.
,
Aborn
,
R. H.
, and
Bain
,
E. C.
,
Metals and Alloys
 0096-7262, Vol.
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,
12
1937
, pp. 345-348.
54.
Hanson
,
K. L.
,
Acta Metallurgica
 0001-6160, Vol.
27
,
04
1979
, pp. 515-521.
55.
Woodhead
,
J. H.
, “
The Statistical Errors in Grain Size Measurement
,”
Quantitative Analysis of Microstructures in Medicine, Biology and Materials Development
,
Riederer-Verlag
,
Stuttgart
,
1975
, pp. 265-276.
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