Skip to Main Content
Skip Nav Destination
ASTM Selected Technical Papers
Fractography in Failure Analysis
By
BM Strauss
BM Strauss
1
Gulf Research and Development Company
,
Pittsburgh, Pa. 15230, editor
Search for other works by this author on:
WH Cullen, Jr Jr
WH Cullen, Jr Jr
2
U.S. Naval Research Laboratory
,
Washington, D.C. 20375, editor
Search for other works by this author on:
ISBN-10:
0-8031-0359-X
ISBN:
978-0-8031-0359-7
No. of Pages:
398
Publisher:
ASTM International
Publication date:
1978

Fracture surfaces, produced by sustained load gaseous hydrogen assisted cracking of 18Ni maraging steel, were examined by scanning electron microscopy. Cracking developed along boundaries associated with the maraging steel microstructure. The specific crack path depended on test temperature and correlated with the influence of this variable on crack growth rates. At low temperatures, crack-growth proceeded predominantly along prior austenite grain boundaries. Increasing temperature produced a continuously increasing amount of transgranular quasicleavage associated with lath martensite boundaries. The proportions of quasicleavage fracture correlated with temperature induced reductions in the crack rate over those predicted from low temperature Arrhenius behavior. Both reduced hydrogen pressure and yield strength decreased the temperature for the onset of the transition to transgranular fracture but had no influence on the crack path. The lower strength steel fracture morphology contained an increased proportion of features typical of ductile rupture. The crack path through the microstructure was independent of the applied stress intensity factor, and hence crack growth rate, from very low values to those beyond the Stage I and Stage II transition for all temperature conditions. Comparison between fractographic observations and known sites for hydrogen segregation suggested that microstructural features play a significant role in the mechanism for gaseous hydrogen embrittlement.

1.
Jewett
,
R. P.
,
Walter
,
R. J.
,
Chandler
,
W. T.
, and
Frohmberg
,
R. P.
, “
Hydrogen Environment Embrittlement of Metals
,” NASA Report CR-2163,
National Aeronautics and Space Administration
, Washington, D.C.,
1973
.
2.
Walter
,
R. J.
and
Chandler
,
W. T.
, “
Influence of Gaseous Hydrogen on Metals
,” NASA Report CR-124410,
National Aeronautics and Space Administration
, Washington, D.C.,
1973
.
3.
Hudak
,
S. J.
, Jr.
, Masters thesis,
Lehigh University
,
1972
.
4.
Gangloff
,
R. P.
, Ph.D. thesis,
Lehigh University
,
1974
.
5.
Dautovich
,
D. P.
and
Floreen
,
S.
in
Proceedings, International Conference on Stress Corrosion Cracking and Hydrogen Embrittlement of Iron Based Alloys
,
Hochmann
J.
,
Slater
J.
, and
Staehle
R. W.
, Eds.,
National Association of Corrosion Engineers
,
Houston, Tex.
1974
, in press.
6.
Sawicki
,
V. R.
, Jr.
, Ph.D. thesis,
Cornell University
,
1971
.
7.
Kerns
,
G. E.
, Ph.D. thesis,
Ohio State University
,
1973
.
8.
Nelson
,
H. G.
and
Williams
,
D. P.
in
Proceedings, International Conference on Stress Corrosion Cracking and Hydrogen Embrittlement of Iron Based Alloys
,
Hochmann
J.
,
Slater
J.
, and
Staehle
R. W.
, Eds.,
National Association of Corrosion Engineers
,
Houston, Tex.
,
1974
, in press.
9.
Troiano
,
A. R.
and
Fidelle
,
J. P.
in
Proceedings, Conference L'Hydrogene Dans Les M'etaux
,
Paris
,
1972
, p. 31.
10.
Gerberich
,
W. W.
,
Chen
,
Y. T.
, and
St. John
,
C.
,
Metallurgical Transactions
 0026-086X, Vol.
6A
,
1975
, p. 1485.
11.
Johnson
,
H. H.
in
Proceedings, International Conference on Stress Corrosion Cracking and Hydrogen Embrittlement of Iron Based Alloys
,
Hochmann
J.
,
Slater
J.
, and
Staehle
R. W.
, Eds.,
National Association of Corrosion Engineers
,
Houston, Tex.
,
1974
, in press.
12.
Beachem
,
C. D.
and
Pelloux
,
R. M. N.
in
Fracture Toughness Testing and Its Applications
, ASTM STP 381,
American Society for Testing and Materials
,
1965
, p. 210.
13.
Fidelle
,
J. P.
,
Legrand
,
J.
, and
Couderc
,
C.
, “
A Fractographic Study of Hydrogen Gas Embrittlement in Steels
,” Paper No. F71-8,
The Metallurgical Society of the American Institute of Mining, Metallurgical, and Petroleum Engineers
,
1971
.
14.
Wei
,
R. P.
and
Landes
,
J. D.
,
Materials Research and Standards
 0025-5394, Vol.
9
,
1969
, p. 25.
15.
Stavros
,
A. J.
and
Paxton
,
H. W.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 3049.
16.
Nelson
,
H. G.
,
Williams
,
D. P.
, and
Tetelman
,
A. S.
,
Metallurgical Transactions
 0026-086X, Vol.
2
,
1971
, p. 953.
17.
Oriani
,
R. A.
and
Josephic
,
P. H.
,
Acta Metallurgica
 0001-6160, Vol.
22
,
1974
, p. 1065.
18.
Dautovich
,
D. P.
and
Floreen
,
S.
,
Metallurgical Transactions
 0026-086X, Vol.
4
,
1973
, p. 2627.
19.
Beachem
,
C. D.
,
Metallurgical Transactions
 0026-086X, Vol.
3
,
1972
, p. 437.
20.
McIntyre
,
P.
in
Proceedings, International Conference on Stress Corrosion Cracking and Hydrogen Embrittlement of Iron Based Alloys
,
Hochmann
J.
,
Slater
J.
, and
Staehle
R. W.
, Eds.,
National Association of Corrosion Engineers
,
Houston, Tex.
,
1974
, in press.
21.
Moon
,
D. M.
and
Landes
,
J. D.
,
Scripta Metallurgia
 0036-9748, Vol.
10
,
1976
, p. 121.
22.
Gangloff
,
R. P.
and
Wei
,
R. P.
,
Metallurgical Transactions
 0026-086X, Vol.
8A
,
1977
, p. 1043.
23.
Pampillo
,
C. A.
and
Paxton
,
H. W.
,
Metallurgical Transactions
 0026-086X, Vol.
3
,
1972
, p. 2895.
24.
Cox
,
T. B.
and
Low
,
J. R.
,
Metallurgical Transactions
 0026-086X, Vol.
5
,
1974
, p. 1457.
25.
Spaeder
,
G. J.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 2011.
26.
Carter
,
C. S.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 1551.
27.
Wayman
,
M. L.
and
Smith
,
G. C.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 1189.
28.
Bernstein
,
I. M.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 3143.
29.
Rath
,
B. B.
and
Bernstein
,
I. M.
,
Metallurgical Transactions
 0026-086X, Vol.
2
,
1971
, p. 2845.
30.
Bernstein
,
I. M.
,
Materials Science and Engineering
 0025-5416, Vol.
6
,
1970
, p. 1.
31.
Krauss
,
G.
and
Marder
,
A. R.
,
Metallurgical Transactions
 0026-086X, Vol.
2
,
1971
, p. 2357.
32.
Roberts
,
M. J.
,
Metallurgical Transactions
 0026-086X, Vol.
1
,
1970
, p. 3287.
33.
Lapasset
,
G.
,
Laurent
,
J. P.
,
Avcouturer
,
M.
, and
Lacombe
,
P.
in
Proceedings, Conference L'Hydrogene Dans Les M'etaux
,
Paris
,
1972
, p. 108.
34.
Laurent
,
J. P.
,
Lapasset
,
G.
,
Avcouturer
,
M.
, and
Lacombe
,
P.
in
Hydrogen in Metals
,
Bernstein
I. M.
and
Thompson
A. W.
, Eds.,
American Society for Metals
,
Metals Park, Ohio
,
1974
, p. 559.
This content is only available via PDF.
You do not currently have access to this chapter.
Close Modal

or Create an Account

Close Modal
Close Modal