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ASTM Selected Technical Papers
Applications of Electron Microfractography to Materials Research
By
W Wiebe
W Wiebe
1
Associate research officer
,
Structures and Materials Laboratory, National Research Council of Canada
,
Ottawa, Ont.,
Canada
;
symposium chairman
.
Search for other works by this author on:
ISBN-10:
0-8031-0746-3
ISBN:
978-0-8031-0746-5
No. of Pages:
102
Publisher:
ASTM International
Publication date:
1971

Because brittle fracture surfaces sometimes carry a clear imprint of the results of prior thermomechanical history of a material, electron fractography can be used to glean information on this history. This is particularly so for those high-temperature phenomena that involve the development of elimination of small holes in solids. Examples of such holes are sintering pores, creep cavities, and gas bubbles. If the matrix is brittle at low temperatures the holes can be exposed for detailed microscopic examination simply by snapping the specimen at low temperature. This requirement is satisfied in tungsten in which we have studied the crystallography and the growth rates of gas bubbles, the morphologies of creep cavities, and the mechanism of hot cracking in fusion welds.

1.
Taylor
,
J. L.
and
Boone
,
D. H.
, “
Tensile Properties of Pyrolytic Tungsten from 1370 to 2980 C in Vacuum
,”
Journal of Less-Common Metals
 0022-5088, Vol.
6
,
1964
, p. 157.
2.
Farrell
,
K.
,
Houston
,
J. T.
, and
Schaffhauser
,
A. C.
, “
The Growth of Grain Boundary Gas Bubbles in Chemically Vapor Deposited Tungsten
,”
Proceedings of Conference on Chemical Vapor Deposition of Refractory Metals, Alloys, and Compounds
,
Gatlinburg, Tenn.
1967
,
American Nuclear Society
, p. 363.
3.
Festa
,
J. V.
and
Danko
,
J. C.
, “
Some Effects of Fluorine Content on the Properties of Chemically Vapor Deposited Tungsten
,”
Proceedings of Conference on Chemical Vapor Deposition of Refractory Metals, Alloys, and Compounds
,
Gatlinburg, Tenn.
,
1967
,
American Nuclear Society
, p. 349.
4.
Koo
,
R. C.
, “
Evidence for Voids in Annealed Doped Tungsten
,”
Transactions, Metallurgical Society, American Institute of Mining, Metallurgical, and Petroleum Engineers
, Vol.
239
,
1967
, p. 1996.
5.
Das
,
G.
and
Radcliffe
,
S. V.
, “
Internal Void Formation in Powder Metallurgy Tungsten
,”
Transactions, Metallurgical Society, American Institute of Mining Metallurgical, and Petroleum Engineers
, Vol.
242
,
1968
, p. 2191.
6.
Farrell
,
K.
,
Houston
,
J. T.
, and
Chumley
,
J. W.
, “
Hot Cracking in Fusion Welds in Tungsten
,”
Welding Journal
, Vol.
35
, No.
3
,
1970
, p. 132s.
7.
Blenkinsop
,
P. A.
and
Morton
,
P. H.
, “
The Influence of Oxygen upon Intergranular Fracture in Cast Tungsten
,”
Journal of the Institute of Metals
 0020-2975, Vol.
96
,
1968
, p. 248.
8.
Farrell
,
K.
,
Loh
,
B.T.M.
, and
Stiegler
,
J. O.
, “
Morphologies of Bubbles and Voids in Tungsten
,”
Transactions of the American Society for Metals
, Vol.
60
,
1967
, p. 485.
9.
Wolfenden
,
A.
and
Farrell
,
K.
, “
Bubble Growth Processes at Grain Boundaries in CVD Tungsten
,”
Journal of Nuclear Materials
 0022-3115, Vol.
29
,
1969
, p. 133.
10.
Stiegler
,
J. O.
,
Farrell
,
K.
,
Loh
,
B. T. M.
, and
McCoy
,
H. E.
, “
Nature of Creep Cavities in Tungsten
,”
Transactions of the American Society for Metals
, Vol.
60
,
1967
, p. 494.
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