Evaluation of Fracture Toughness of X100 Pipe Steel Using SE(B) and Clamped SE(T) Single Specimens Available to Purchase

J-resistance testing using a single-specimen unloading compliance technique has been performed on single-edge-notched tension (SE(T)) specimens of X100 pipe steel base material at room temperature and at −20°C, using a procedure developed at CANMET. J-resistance testing using single-edge-notched bend (SE(B)) specimens according to ASTM E1820 was also conducted for comparison. The specimens included two nominal through-thickness pre-crack aspect ratios (a/W = 0.25 and 0.5). The results show that shallow-cracked (a/W∼0.25) bend and tension specimens produce higher resistance curves than deeply-cracked (a/W∼0.5) specimens; ductile propagation was observed at both temperatures. Resistance curves are slightly higher at −20°C than at room temperature for both bending and tension, especially for shallow-cracked specimens. Crack length predicted from unloading compliance of crack mouth opening displacement for the SE(T) specimens was validated by optical measurement of initial crack length (a_o) and final crack extension (Δa>1.0 mm) after heat-tinting, as per ASTM E1820. Predicted crack growths show acceptable agreement with measured values in all cases. The effect of side-groove depth on the resistance curve and straightness of the crack front was briefly investigated. For both bending and tension, resistance curves for 10% (total) side-grooved specimens were close to those from plain-sided specimens when other testing conditions, such as precrack and testing temperature, were the same, whereas 20% (total) side-grooved specimens showed lower toughness. It was occasionally observed that the crack grew faster at the side for 20% side-grooved bend and tension specimens, resulting in a crack front of concave curvature. For 10% side-grooved specimens a rather straight crack front or slightly faster crack growth in the middle of the specimen (convex curvature) was observed.