Testing of catalytic converter with exhaust gas re-circulation system for diesel engine to reduce pollute gases is chosen for present work. The emphasis is given on hydrocarbon (HC), carbon monoxide (CO) and oxides of nitrogen. The catalytic converter was developed with variations of catalyst plates. Perforated plates of copper and combination of copper oxide and cerium oxide (CeO2 +CuO) were used as the catalyst. Copper spacer was used in between plates to vary the distance. Secondary air was injected into the converter to aid oxidization of HC and CO. Experimental study was carried out on computerized kirloskar single cylinder four stroke (10 B.H.P, 7.4 KW) diesel engine test rig with an eddy current dynamometer. The converter was tested with various combination with exhaust gas re-circulation (EGR) system. There are some improvements in the reduction and conversion efficiency of HC & CO. Exhaust gas re-circulation has proved to be effective in reducing NOx.

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