Nanostructured MoSi2 powder has been successfully synthesized by Ball milling of Mo and Si powder mixtures and subsequent self-propagating high-temperature synthesis (SHS) process. It was observed that in comparison with the normally mixed powder, it could be easily ignited and higher combustion temperature was achieved. Based on XRD and SEM, it was confirmed that nanostructure MoSi2 powder could be prepared through self propagating combustion method from the mechanical activated powder mixture.

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